Optimization of Extraction Technology for Total Phenolic Acids from Fruits by Central Composite Design-response Surface Methodology

doi:10.13422/j.cnki.syfjx.2014180030

您当前的位置：

首页 >

文章列表页 >

Optimization of Extraction Technology for Total Phenolic Acids from Fruits by Central Composite Design-response Surface Methodology

更新时间：2024-01-04

- Optimization of Extraction Technology for Total Phenolic Acids from Fruits by Central Composite Design-response Surface Methodology
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 18, Pages: 30-33(2014)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2014180030
  CLC： R284.2
- Published：2014
- 稿件说明：
移动端阅览
Optimization of Extraction Technology for Total Phenolic Acids from Fruits by Central Composite Design-response Surface Methodology[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(18): 30-33.
DOI：

Optimization of Extraction Technology for Total Phenolic Acids from Fruits by Central Composite Design-response Surface Methodology[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(18): 30-33. DOI： 10.13422/j.cnki.syfjx.2014180030.

摘要

目的：优选维吾尔药刺山柑果总酚酸的提取工艺。方法：采用乙醇回流提取法，通过单因素试验确定提取次数，以乙醇体积分数、溶剂用量、提取时间为自变量，总酚酸提取量为因变量，通过对自变量各水平的多元线性回归及二项式拟合，利用响应面法优选刺山柑果总酚酸的提取工艺并进行预测分析。结果：最佳提取工艺为加15倍量70%乙醇提取2次，每次1 h；总酚酸提取量7.29 mg·g-1，与模型预测值（7.34 mg·g-1）的相对标准偏差0.68%。结论：星点设计-响应面法优选的刺山柑果总酚酸提取工艺简单、精密度高、可预测性好。

Abstract

Objective: To optimize extraction process of total phenolic acids in Capparis spinosa fruits. Method: Independent variables were ethanol concentration

solvent amounts and extracting time

dependent variable was yield of total phenolic acids

levels of independent variables were regressed multiple linearity and fitted by binomial

response surface methodology was used to optimize extraction process

then compared both of observed and predicted values. Result: Optimum extraction progress was as follows:extracted 2 twice with 15 times the amount of 70% ethanol for 1 h per time;yield of total phenolic acids was 7.29 mg·g-1

whose deviation was 0.68% by comparing with the predicated value(7.34 mg·g-1). Conclusion: This optimized process was simple with high precision and good predictability.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Determination of Protocatechuic Acid and Protocatechualdehyde in Feiyanping Capsule by HPLC

Study on Dynamics Trends of Protocatechuic Acid Content of the Rupr. in Different Growth Stages

Determination of Protocatechuic Acid, Chlorgenic Acid and Caffeic Acid in Sangye Dispensing Granules by HPLC

Studies on Separation and Purification of Total Phenolic Acids from Salvia by Polyamide Resins

Related Author

XING Jun-bo1

WANG Zhao-hong2

ZHANG Shu-rong

PEI Miao-rong

PEI Xiang-ping

HUANG Can-lin

HUANG Xuan

Wang Qin

Related Institution

Shaanxi Traditional Chinese Medicine

Zhangye Institute for Drug Control

Zhangye Medical College

Shanxi College of Traditional Chinese Medicine

山西中医学院山西太原030024

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰