Analysis of Volatile Constituents of by GC-MS

LU Kuan; LI Ming; LI Feng; CUI Wei; WANG Qiao-rong; LIU Jian-hua

doi:10.13422/j.cnki.syfjx.2014190053

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Analysis of Volatile Constituents of by GC-MS

更新时间：2024-01-04

- Analysis of Volatile Constituents of by GC-MS
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 19, Pages: 53-56(2014)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2014190053
  CLC： R284.1
- Published：2014
- 稿件说明：
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LU Kuan, LI Ming, LI Feng, et al. Analysis of Volatile Constituents of by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(19): 53-56.
DOI：

LU Kuan, LI Ming, LI Feng, et al. Analysis of Volatile Constituents of by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(19): 53-56. DOI： 10.13422/j.cnki.syfjx.2014190053.

摘要

目的：分析泰国大风子的挥发性成分，为泰国大风子的开发利用提供实验依据。方法：利用水蒸气蒸馏法提取泰国大风子挥发油，采用气相色谱-质谱联用（GC-MS）技术对挥发油进行分析，HP-5MS 5% Phenyl Methyl Siloxane弹性石英毛细管柱（0.25 μm×250 μm×30 m），进样量1 μL，气化室温度250 ℃，柱温50 ℃，保持2 min，然后以4 ℃·min-1升温至230 ℃，保持20 min，柱前压15.08 psi，载气流量2.0 mL·min-1；载气为高纯度氦气（99.999%），分流比40：1。结果：共分离出63个化学成分，对其中49个化学成分进行了鉴别，占挥发油总量的93.48%。其主要成分为1，8-桉树油（17.28%），茴香烯（9.28%），异硫氰酸丙酯（7.76%），双环[7.1.0]癸烷（4.73%），丹皮酚（3.25%）。结论：本文采用气相色谱-质谱联用法对泰国大风子的挥发性成分进行研究，为该植物的深度开发提供参考。

Abstract

Objective: This study aimed To analyze the volatile constituents of Hydnocarpus anthelminthica to provide the foundation of reasonable utilization of this herb. Method: The volatile oil was extracted from H. anthelminthica by team distillation. The chemical constituents were analyzed by GC-MS. Result: Sixty-three compounds were separated and 49 of them were identified

which accounted for 93.48% of all the volatile oil. The major components were 1

8-cineole (17.28%)

trans-anethole (9.28%)

1-isothiocyanato-propane (7.76%)

bicyclo[7.1.0]decane (4.73%)

peonol (3.25%). Conclusion: The volatile oil of H. anthelminthica was extracted by team distillation and analyzed by GC-MS.

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Related Institution

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