Chemical Constituents of Physalis Calyx Seu Fructus

SHU Zun-peng; XU Bing-qing; XING Na; LI Xin-li; WANG Qiu-hong; YANG Bing-you; KUANG Hai-xue

doi:10.13422/j.cnki.syfjx.2014210099

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Chemical Constituents of Physalis Calyx Seu Fructus

更新时间：2024-01-04

- Chemical Constituents of Physalis Calyx Seu Fructus
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 21, Pages: 99-102(2014)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2014210099
  CLC： R284.1;R284.2
- Published：2014
- 稿件说明：
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SHU Zun-peng, XU Bing-qing, XING Na, et al. Chemical Constituents of Physalis Calyx Seu Fructus[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(21): 99-102.
DOI：

SHU Zun-peng, XU Bing-qing, XING Na, et al. Chemical Constituents of Physalis Calyx Seu Fructus[J]. Chinese journal of experimental traditional medical formulae, 2014, 20(21): 99-102. DOI： 10.13422/j.cnki.syfjx.2014210099.

摘要

目的: 研究锦灯笼的化学成分。方法: 采用硅胶、ODS柱色谱、Sephadex LH-20和半制备液相色谱等技术分离纯化

结合ESI-MS

NMR等现代波谱学技术进行结构鉴定。结果: 分离并鉴定了8个化合物

分别为(+)-丁香脂素-O-β-D-双吡喃葡萄糖苷(1)

(+)-松脂酚-O-β-D-双吡喃双葡萄糖苷(2)

(+)-杜仲树脂酚-O-β-D-双吡喃葡萄糖苷(3)

芹菜素-7-O-β-D-葡萄糖苷(4)

金圣草黄素-7-O-β-D-葡萄糖苷(5)

香叶木素-7-O-β-D-葡萄糖苷(6)

莨菪亭-7-O-β-D-葡萄糖苷(7)和对羟基苯乙醇-(阿魏酸-4-O-β-D-葡萄糖酯)苷(8)。结论: 化合物1~8均为首次从该植物中分离得到。

Abstract

Objective: To study the chemical constituents from Physalis Calyx Seu Fructus. Method: The chemical constituents were isolated and purified by silica gel

ODS column chromatography

Sephadex LH-20 and semi-preparing HPLC. Their structures were identified on the basis of ESI-MS

UV and NMR spectra. Result: Eight compounds were isolated and elucidated as (+)-syringaresinol-O-β-D-di-glucopyranoside (1)

(+)-pinoresinol-O-β-D-di-glucopyranoside (2)

(+)-medioresinol-O-β-D-di-glucopyranoside (3)

apigenin-7-O-β-D-glucoside (4)

chrysoeriol-7-O-β-D-glucoside (5)

diosmetin-7-O-β-D-glucoside (6)

scopoletin-7-O-β-D-glucoside (7) and syringalide B (8). Conclusion: Compounds 1-8 were firstly obtained from this plant.

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