Chemical Constituents Occurring in Roots of

LIU Ai-hong; HU Zhi-cheng; REN Gang; YUAN Jin-bin; YI Wen-fang; PENG Jia-bing; YUAN Wen-jun

doi:10.13422/j.cnki.syfjx.2014220091

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Chemical Constituents Occurring in Roots of

更新时间：2024-01-04

- Chemical Constituents Occurring in Roots of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 22, Pages: 91-94(2014)
- 作者机构：
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- DOI：10.13422/j.cnki.syfjx.2014220091
  CLC： R284.1
- Published：2014
- 稿件说明：
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LIU Ai-hong, HU Zhi-cheng, REN Gang, et al. Chemical Constituents Occurring in Roots of [J]. Chinese journal of experimental traditional medical formulae, 2014, 20(22): 91-94.
DOI：

LIU Ai-hong, HU Zhi-cheng, REN Gang, et al. Chemical Constituents Occurring in Roots of [J]. Chinese journal of experimental traditional medical formulae, 2014, 20(22): 91-94. DOI： 10.13422/j.cnki.syfjx.2014220091.

摘要

目的: 研究南川木波罗根皮的化学成分.方法: 采用硅胶、Diaion HP20大孔吸附树脂、MCI gel CHP 20P树脂凝胶、Sephadex LH-20凝胶、ODS等柱色谱分离手段

对南川木波罗根皮醇提物的乙酸乙酯部位进行化学成分的分离纯化

根据化合物的理化性质及光谱数据鉴定其结构.结果: 分离了9个化合物

分别鉴定为4-羟基苯甲醛(p-hydroxybenzaldehyde)(1)

4-二羟基苯甲酸(2

4-dihydroxybenzoic acid)(2)

香豆酸 (p-coumaric acid)(3)

儿茶素[(+) catechin](4)

(E)-阿魏酸甲酯[(E)-ferulic acid methyl ester](5)

E-对-羟基肉桂酸甲酯(p-E-hedroxycinnamic acid methyl ester)(6)

norartocarpetin(7)

反式氧化白黎芦醇(trans-oxyresveratrol)(8)

moracin M(9).结论: 化合物1

6为首次从桑科植物中获得

化合物3为首次在波罗蜜属植物中发现

而化合物7~9为首次从南川木波罗中分离得到.

Abstract

Objective:To study the chemical constituents of roots of Artocarpus nanchuanensis. Method: The constituents were isolated from the ethyl acetate portion of 95% ethanol extraction of A. nanchuanensis roots by column chromatography over silica gel

Diaion HP20 macroreticular resin

MCI CHP 20P gel

Sephadex LH-20 gel

ODS gel

etc. Their structures were elucidated by analysis of physical chemical properties and spectral data. Result: Nine compounds were isolated and their structures were identified as p-hydroxybenzaldehyde(1)

4-dihydroxybenzoic acid(2)

p-coumaric acid(3)

(+) catechin(4)

(E)-ferulic acid methyl ester(5)

p-E-hedroxycinnamic acid methyl ester(6)

norartocarpetin(7)

trans-oxyresveratrol(8)

moracin M(9). Conclusion: Compounds 1

5 and 6 were isolated from Moraceae for the first time. Compound 3 was firstly reported the occurrence in the genus Artocarpus

and compounds 7-9 were characterized in A. nanchuanensis for the first time.

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