Chemical Compositions of

SHI Yu; MA Yang-min; KANG Yong-xiang; WANG Ning-hui

doi:10.13422/j.cnki.syfjx.2014230104

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Chemical Compositions of

更新时间：2024-01-04

- Chemical Compositions of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 20, Issue 23, Pages: 104-106(2014)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2014230104
  CLC： R284.1
- Published：2014
- 稿件说明：
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SHI Yu, MA Yang-min, KANG Yong-xiang, et al. Chemical Compositions of [J]. Chinese journal of experimental traditional medical formulae, 2014, 20(23): 104-106.
DOI：

SHI Yu, MA Yang-min, KANG Yong-xiang, et al. Chemical Compositions of [J]. Chinese journal of experimental traditional medical formulae, 2014, 20(23): 104-106. DOI： 10.13422/j.cnki.syfjx.2014230104.

摘要

目的: 研究太白山地区美丽芍药Paeonia mairei的化学成分

为其药理研究与作用机制提供依据. 方法: 采用硅胶柱色谱、Sephadex LH-20凝胶柱色谱、重结晶等方法分离纯化化合物

并通过化合物的理化性质和波谱分析鉴定其结构. 结果: 从美丽芍药中分离得到8个化合物

分别为β-谷甾醇(1)

齐墩果酸(2)

常春藤皂苷元(3)

胡萝卜苷(4)

大黄酚(5)

苯甲酸(6)

没食子酸(7)

没食子酸乙酯(8). 结论: 化合物5为从该属植物中首次分离得到

其余化合物均为首次从该植物中得到.

Abstract

Objective: To study the chemical constituents of Paeonia mairei in Taibai mountains and to supply material basis for its pharmacological research and therapeutic mechanism. Method: The compounds from P. mairei were isolated and purified by silica gel column chromatography

Sephadex LH-20 column chromatography and recrystallization method

and their structures were elucidated on the basis of their physicochemical properties and spectra analysis. Result: Eight compounds were obtained and identified as β-sitosterol(1)

oleanic acid(2)

hederagenin(3)

daucosterol(4)

chrysophanol(5)

benzoic acid(6)

gallic acid(7)

ethyl gallate(8). Conclusion: Compound 5 were obtained from the genus for the first time. The rest of the compounds was isolated from the plant of P. mairei for the first time.

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Related Institution

Key Laboratory for Standardization of Chinese Medicines，Ministry of Education， Shanghai Key Laboratory for Compound Chinese Medicines，Institute of Chinese Materia Medica， Shanghai University of Traditional Chinese Medicine

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Institute of Chinese Materia Medica，China Academy of Chinese Medical Sciences

School of TCM,Guangdong Pharmaceutical University

Key Laboratory of Basic and Applied Research of Northern Medicine,Ministry of Education,Heilongjiang Key Laboratory of Pharmacodynamic Material Basis of Traditional Chinese Medicine (TCM) and Natural Medicine,Heilongjiang University of Chinese Medicine

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