LI Shu-ying, LI Xiao-fei, CHEN Fei, et al. Optimization of Purification Technology for Evodiamine from Euodiae Fructus by Macroporous Resin[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(4): 27-29.
DOI:
LI Shu-ying, LI Xiao-fei, CHEN Fei, et al. Optimization of Purification Technology for Evodiamine from Euodiae Fructus by Macroporous Resin[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(4): 27-29. DOI: 10.13422/j.cnki.syfjx.2015040027.
Optimization of Purification Technology for Evodiamine from Euodiae Fructus by Macroporous Resin
Objective: To optimize separation and purification technology conditions of evodiamine from ethanol extract of Euodiae Fructus by macroporous resin. Method: With adsorption volume and elution rate of evodiamine as indexes
five kinds(AB-8
S-8
NKA-9
HPD-100
D-101) of macroporous resins were selected by static adsorption and desorption test.Sample solution concentration
sample volume
sample flow rate
eluent type
eluent amount and other parameters were investigated by single factor tests. Result: D-101 macroporous resin had the best separation and purification capacity for evodiamine in following technology conditions:sample concentration of 3 g · L-1
sample volume of 4 BV
sample flow rate of 1 BV · h-1
removed water-soluble impurities with 5 BV of water
eluted with 5 BV of 80% ethanol
eluting velocity of 2 BV · h-1.Elution rate of evodiamine was 92.81%
its purity increased from 1.29% to 26.77%. Conclusion: D-101 macroporous resin is suitable for purifying evodiamine from Euodiae Fructus.This optimized method is stable and feasible
it can provide a reference for development and utilization of evodiamine.
Optimization of Separation and Enrichment Process of Iridoid Glycosides from Lonicerae Japonicae Flos by Macroporous Resin
Pharmacokinetics of Euodiae Fructus Powder Dressing on Foot Sole of Japanese Big-ear Rabbits with Vinegar
Transdermal Effect of Euodiae Fructus Oil-in-water Microemulsion Cataplasm
Fingerprint and Content Determination of Euodiae Fructus Collected in Guizhou and Zhejiang
Hepatotoxicity and Anti-osteoporotic Mechanism of Evodiamine
Related Author
ZHANG Yu
YANG Jian
QIN Zhen-xian
QI Meng-die
ZHANG Quan
LIU Shuang
LIU Yong
YUAN Yuan
Related Institution
Beijing Key Laboratory for Quality Evaluation of Chinese Materia Medical/Traditional Chinese Medicine(TCM) Processing Technology Inheritance Base of National Administration of TCM, School of Chinese Materia Medica, Beijing University of Chinese Medicine
Wangjing Hospital, China Academy of Chinese Medical Sciences
Guizhou Provincial Key Laboratory of Pharmaceutics,Guizhou Medical University
Institute of Chinese Materia Medica,China Academy of Chinese Medical Sciences
Guang′anmen Hospital,China Academy of Chinese Medical Sciences