Chemical Composition of Ethyl Acetate Fraction of Notoginseng Radix et Rhizoma Medicinal Fungal

DING Cai-feng; WANG Ming-jiao; QIU Zhi-dong; XU Wei

doi:10.13422/j.cnki.syfjx.2015070043

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Chemical Composition of Ethyl Acetate Fraction of Notoginseng Radix et Rhizoma Medicinal Fungal

更新时间：2024-09-23

- Chemical Composition of Ethyl Acetate Fraction of Notoginseng Radix et Rhizoma Medicinal Fungal
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 21, Issue 7, Pages: 43-46(2015)
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- DOI：10.13422/j.cnki.syfjx.2015070043
  CLC： R284.1
- Published：2015
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DING Cai-feng, WANG Ming-jiao, QIU Zhi-dong, et al. Chemical Composition of Ethyl Acetate Fraction of Notoginseng Radix et Rhizoma Medicinal Fungal[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(7): 43-46.
DOI：

DING Cai-feng, WANG Ming-jiao, QIU Zhi-dong, et al. Chemical Composition of Ethyl Acetate Fraction of Notoginseng Radix et Rhizoma Medicinal Fungal[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(7): 43-46. DOI： 10.13422/j.cnki.syfjx.2015070043.

摘要

目的: 研究三七药性菌质的乙酸乙酯层化学成分。方法: 采用系统溶剂萃取、薄层色谱、硅胶柱色谱、半制备型HPLC色谱等方法进行分离纯化

通过化学性质和波谱数据确定化合物的结构。结果: 从三七药性菌质的乙酸乙酯层中分离得到6个化合物

分别为20(S)-人参皂苷Rh1(1)

20(R)-人参皂苷Rh1(2)

人参皂苷F1(3)

24(S)-拟人参皂苷F11(4)

23-二脱氢拟人参皂苷RT4(5)

5α-麦角甾-7

22-二烯-3β

6β-三醇(6)。结论: 化合物 5 为新化合物

命名为拟人参皂苷RT7

化合物 4

6 为首次从三七中分离得到

化合物 1～6 均为首次从三七药性菌质中分离得到。

Abstract

Objective: Aim to study the chemical constituents of the ethyl acetate fraction of Notoginseng Radix et Rhizoma medicinal fungal. Method: The compounds were separated and purified by the system solvent extraction

thin-layer chromatography

column chromatography on silica gel

semi-preparative liquid chromatography. Their structures were determined by comparison of their chemical properties and spectral data with those of the authentic samples and those reported in the literatures. Result: Six compounds were separated and identified as 20(S)-ginsenoside Rh1(1)

20(R)-ginsenoside Rh1(2)

ginsenoside F1(3)

24(S)-pseudoginsenoside F11(4)

23-didehydropseudoginsenoside RT4(5)

5α-ergosta-7

22-diene-3β

6β-triol (6). Conclusion: Compound 5 was a new compound

named pseudoginsenoside RT7

and compounds 4 and 6 were isolated from Notoginseng for the first time

and all compounds were isolated from Notoginseng Radix et Rhizoma medicinal fungale for the first time.

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