Quality Standard for Boiled Powder of Maxing Erchen Tang

LIU Qian; CHEN Jin-yue; WEN Jun; LAN Chuan-yan

doi:10.13422/j.cnki.syfjx.2015090071

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Quality Standard for Boiled Powder of Maxing Erchen Tang

更新时间：2024-01-04

- Quality Standard for Boiled Powder of Maxing Erchen Tang
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 21, Issue 9, Pages: 71-73(2015)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2015090071
  CLC： O657.7;R286.0
- Published：2015
- 稿件说明：
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LIU Qian, CHEN Jin-yue, WEN Jun, et al. Quality Standard for Boiled Powder of Maxing Erchen Tang[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(9): 71-73.
DOI：

LIU Qian, CHEN Jin-yue, WEN Jun, et al. Quality Standard for Boiled Powder of Maxing Erchen Tang[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(9): 71-73. DOI： 10.13422/j.cnki.syfjx.2015090071.

摘要

目的: 建立麻杏二陈汤煮散质量标准. 方法: 采用薄层色谱法(TLC)对煮散处方中的炙麻黄、苦杏仁、射干、陈皮进行定性鉴别

采用高效液相色谱法(HPLC)对煮散中的射干苷和橙皮苷含量进行同时测定. 结果: TLC法能定性检出炙麻黄、苦杏仁、射干、陈皮

斑点清晰

且阴性对照无干扰.HPLC法测定射干苷在12.0～120.0 mg·L-1呈良好的线性关系(r=0.999 8)

平均回收率100.00%(RSD 1.9%);橙皮苷在6.6～66.0 mg·L-1呈良好的线性关系(r=0.999 9)

平均回收率98.16%(RSD 1.8%). 结论: 该研究所建立的定性、定量检测方法操作简便

结果准确可靠

重复性好

能有效地控制麻杏二陈汤煮散的质量.

Abstract

Objective: To establish the quality standard for boiled powder of Maxing Erchen Tang. Method: The qualitative identifications of honey-fried Ephedrae Herba

Armeniacae Semen Amarum

Belamcandae Rhizoma and Citri Reticulatae Pericarpium were carried out by TLC

and the contents of belamcandin and hesperidin were determined by HPLC. Result: The results of TLC showed that the relevant spots were clear without interference in the blank reference. The liner ranges of belamcandin and hesperidin were 12.0-120.0 mg·L-1 (r=0.999 8) and 6.6-66.0 mg·L-1 (r=0.999 9)

respectively. The average recovery of belamcandin was 100.00% with RSD of 1.9%. The average recovery of hesperidin was 98.16% with RSD of 1.8%. Conclusion: The established qualitative and quantitative methods are simple and accurate

reliable and reproducible

and can be effectively used for the quality control of boiled powder of Maxing Erchen Tang.

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