Isolation and Structural Identification of Chemical Constituents from Aurantii Fructus

DENG Ke-zhong; DING Yi-qiang; ZHOU Bin; XIONG Ying; CHEN Hong

doi:10.13422/j.cnki.syfjx.2015140036

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Isolation and Structural Identification of Chemical Constituents from Aurantii Fructus

更新时间：2024-01-04

- Isolation and Structural Identification of Chemical Constituents from Aurantii Fructus
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 21, Issue 14, Pages: 36-38(2015)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2015140036
  CLC： R284.1
- Published：2015
- 稿件说明：
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DENG Ke-zhong, DING Yi-qiang, ZHOU Bin, et al. Isolation and Structural Identification of Chemical Constituents from Aurantii Fructus[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(14): 36-38.
DOI：

DENG Ke-zhong, DING Yi-qiang, ZHOU Bin, et al. Isolation and Structural Identification of Chemical Constituents from Aurantii Fructus[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(14): 36-38. DOI： 10.13422/j.cnki.syfjx.2015140036.

摘要

目的: 研究枳壳中化学成分。方法: 采用硅胶、羟丙基葡聚糖凝胶

ODS柱色谱法进行分离纯化

根据理化性质和波谱数据进行结构鉴定。结果: 从枳壳乙醇提取物中分离得到9个化合物

分别鉴定为伞形花内酯(1)

马尔敏(2)

7'-二羟基香柠檬素(3)

佛手酚(4)

水合橙皮内酯(5)

阿魏酸(6)

柠檬苦素(7)

胡萝卜苷棕榈酸酯(8)

胡萝卜苷(9)。结论: 化合物 3~4

8~9 均为首次从该植物中分离得到。

Abstract

Objective: To investigate the chemical constituents of Aurantii Fructus. Method: The chemical constituents were isolated by chromatography on silica gel

sephadex LH-20 and ODS columns. Their physicochemical properties and spectral data were used to elucidate the structures. Result: Nine compounds were isolated from the ethanol extract of Aurantii Fructus and their structures were identified as umbelliferone (1)

marmin (2)

7'-dihydroxybergamottin (3)

bergaptol (4)

meranzin hydrate (5)

ferulic acid (6)

limonin (7)

daucosterolpalmitate (8)

and daucosterol (9). Conclusion: Compounds 3-4

and 8-9 were isolated from this plant for the first time.

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