Optimization of Percolation Extraction Process of Shexiang Shuhuoling

CUI Long; LU Peng; CAO Li-hua; SHANG Qiang; CAO Hui; GAO Jin

doi:10.13422/j.cnki.syfjx.2015200041

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Optimization of Percolation Extraction Process of Shexiang Shuhuoling

更新时间：2024-01-04

- Optimization of Percolation Extraction Process of Shexiang Shuhuoling
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 21, Issue 20, Pages: 41-43(2015)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2015200041
  CLC： R284.2
- Published：2015
- 稿件说明：
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CUI Long, LU Peng, CAO Li-hua, et al. Optimization of Percolation Extraction Process of Shexiang Shuhuoling[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(20): 41-43.
DOI：

CUI Long, LU Peng, CAO Li-hua, et al. Optimization of Percolation Extraction Process of Shexiang Shuhuoling[J]. Chinese journal of experimental traditional medical formulae, 2015, 21(20): 41-43. DOI： 10.13422/j.cnki.syfjx.2015200041.

摘要

目的:优选麝香舒活灵的渗漉提取工艺

为该制剂的工业化生产工艺改进提供参考。方法:在单因素试验基础上

以梓醇转移率及含固量为综合评价指标

乙醇体积分数、乙醇用量、渗漉速度、药材浸渍时间为考察因素

采用L9(34)正交试验优选麝香舒活灵的渗漉提取工艺。结果:最佳提取工艺条件为加15倍量50%乙醇浸渍6 h

流速0.25 mL·min-1。羟基红花黄色素A和梓醇的转移率分别为97.50%

102.07%

RSD分别为5.4%

3.5%。结论:该工艺提取率及有效成分转移率高

简单易行

适合麝香舒活灵的工业化大生产。

Abstract

Objective: To optimize percolation extraction process of Shexiang Shuhuoling

and provide a reference for process improvement of this preparation in industrial production. Method: Based on single factor test

with composite score of transferring rate of catalpol and solid-containing content as index

orthogonal experimental design was adopted to optimize percolation extraction process by taking percolation rate

immersion time

ethanol concentration and amount as factors. Result: Optimum percolation extraction process was added 15 times the amount of 50% ethanol for immersing 6 h

percolation rate of 0.25 mL·min-1.Transferring rates of hydroxy safflower yellow A and catalpol were 97.50% and 102.07% with RSD of 5.4% and 3.5%

respectively. Conclusion: This process is feasible and economical

which is suitable for industrial production of Shexiang Shuhuoling.

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Related Institution

College of Pharmaceutical Sciences， Southwest University

College of Chemistry and Chemical Engineering Yan’an University,Yan’an

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Henan Collenge of Traditional Chinese Medicine

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