Isolation and Structure Identification of Flavonoid Glycosides in

PAN Zheng-hong; YAN Dong-lan; NING De-sheng; GU Zhi-xin; LI Dian-peng; HUANG Sheng; LIU Jin-lei

doi:10.13422/j.cnki.syfjx.2015240026

您当前的位置：

首页 >

文章列表页 >

Isolation and Structure Identification of Flavonoid Glycosides in

更新时间：2024-09-23

- Isolation and Structure Identification of Flavonoid Glycosides in
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 21, Issue 24, Pages: 26-29(2015)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2015240026
  CLC： R284.1
- Published：2015
- 稿件说明：
移动端阅览
PAN Zheng-hong, YAN Dong-lan, NING De-sheng, et al. Isolation and Structure Identification of Flavonoid Glycosides in [J]. Chinese journal of experimental traditional medical formulae, 2015, 21(24): 26-29.
DOI：

PAN Zheng-hong, YAN Dong-lan, NING De-sheng, et al. Isolation and Structure Identification of Flavonoid Glycosides in [J]. Chinese journal of experimental traditional medical formulae, 2015, 21(24): 26-29. DOI： 10.13422/j.cnki.syfjx.2015240026.

摘要

目的:研究裸花紫珠95%乙醇提取物的化学成分。方法:采用硅胶

MCI

C18等柱色谱方法对裸花紫珠中化学成分进行分离纯化

并经波谱数据分析和文献对照鉴定化合物结构。结果:从裸花紫珠叶95%乙醇提取物中分离得到8个化合物

分别鉴定为木犀草苷(1)

木犀草素-3'-O-β-D-吡喃葡萄糖苷(2)

木犀草素-4'-O-β-D-吡喃葡萄糖苷(3)

芹菜素-7-O-β-D-葡萄糖醛酸苷丁酯(4)

木犀草素-3'-O-(6″-E-咖啡酰)-β-D-吡喃葡萄糖苷(5)

木犀草素-4'-O-(6'-E-咖啡酰)-β-D-吡喃葡萄糖苷(6)

木犀草素-7-O-(6″-E-咖啡酰)-β-D-吡喃葡萄糖苷(7)

木犀草素-7-O-(6″-E-阿魏酰)-β-D-吡喃葡萄糖苷(8)。结论:化合物4为首次从该植物分离得到。

Abstract

Objective: To study the chemical constituents of 95% ethanol extract of Callicarpa nudiflora. Method: The compounds were separated and purified by silica gel

MCI

and C18 column chromatography

while their structures were identified by analyzing their spectral data and comparing with the previously reported literatures. Result: Eight compounds were isolated from 95% ethanol extract of C. nudiflora and their structures were respectively identified as luteoloside(1)

dracocephaloside(2)

juncein(3)

apigenin-7-O-β-D-glucuronide buthyl ester(4)

luteolin-3'-O-(6″-E-caffeoyl)-β-D-glucopyranoside(5)

luteolin-4'-O-β-D-(6″-E-caffeoyl)-glucopyranoside(6)

luteolin-7-O-(6″-E-caffeoyl)-β-D-glucopyranoside(7)

luteolin-7-O-(6″-E-feruloyl)-β-D-glucopyranoside(8). Conclusion: Compound 4 was isolated from this plant for the first time.

关键词

Keywords

references

Views

下载量

CSCD

Alert me when the article has been cited

提交

Tools

Publicity Resources

Identification of Chemical Constituents of Bidens pilosa and Analysis of Its Anti-gastric Cancer Cell Proliferation Activity in Vitro

Chemical Constituents， Pharmacological Activities， and Identification of Amomi Fructus： A Review

Analysis of Material Basis of Famous Classical Formula Baoyuantang Based on UPLC-Q-TOF-MS/MS

Medicinal Resources， Chemical Constituents， and Pharmacological Activities of Salvia Genus： A Review

Chemical Constituents， Pharmacological Effect， and Product Development of Eucommia ulmoides with Both Medicinal and Edible Values： A Review

Related Author

HAN Yu

LIU Chang

LIU Jiao

ZHANG Tao

ZOU Zhongmei

GU Yuancong

TAN Zhihao

LYU Bangyu

Related Institution

Shenyang Pharmaceutical University

Institute of Medicinal Plant Development，Chinese Academy of Medical Sciences&Peking Union College

Henan University of Chinese Medicine

School of Food Science and Engineering，Guangdong Ocean University

School of Materials Science and Engineering，Guangdong Ocean University

AI问答

Postal code：100700
Tel：010-84076882 Email：syfjx_2010@188.com
Technical support is provided by Beijing Founder electronics co., LTD 京ICP备11006657号-10 京公网安备11010802024621
It is recommended to read the content of this site in Chrome&IE9+. Please switch to extreme mode in browser 360.
Cookies We use cookies to help provide and enhance our service and tailor content. By continuing, you agree to the use of cookies.

⁰