Chemical Constituents from Whole Plants of  (IV)

YANG Li-hua; LI Chun; LIN Li-mei; WANG Zhi-min; LI Zhong

doi:10.13422/j.cnki.syfjx.2016040039

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Chemical Constituents from Whole Plants of (IV)

更新时间：2024-01-04

- Chemical Constituents from Whole Plants of (IV)
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 22, Issue 4, Pages: 39-44(2016)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2016040039
  CLC： R29
- Published：2016
- 稿件说明：
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YANG Li-hua, LI Chun, LIN Li-mei, et al. Chemical Constituents from Whole Plants of (IV)[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(4): 39-44.
DOI：

YANG Li-hua, LI Chun, LIN Li-mei, et al. Chemical Constituents from Whole Plants of (IV)[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(4): 39-44. DOI： 10.13422/j.cnki.syfjx.2016040039.

摘要

目的: 研究藏族药甘青乌头全草的化学成分。方法: 采用多种现代色谱技术进行分离纯化

并通过理化性质、波谱分析(1D

2D-NMR和MS)及与文献对比的方法进行结构鉴定。结果: 分离并鉴定了17个化合物

分别为异光黄素(1)

对羟基桂皮酸(2)

苯甲酸(3)

对羟基苯乙胺(4)

对羟基苯乙醇(5)

尼泊金丁酯(6)

腺苷(7)

3-[p-hydroxyphenyl]-propionic acid amide(8)

hetisine(9)

关附辛素(10)

红景天苷(11)

环(异亮-亮)二肽(12)

苯丙氨酸(13)

3-(4-aminophenyl)prop-2-enoic acid(14)

N-oxide hordenine(15)

(2R

3R)-2

4-三羟基丁酸(16)和N-甲基酪胺(17)。结论: 其中化合物 1~4

6~8和12~17 为首次从甘青乌头中分离得到。

Abstract

Objective: To study the chemical constituents from Aconitum tanguticum. Method: The chemical constituents were isolated and purified by using a combination of modern chromatographic techniques

and their structures were determined through spectral analysis(1D

2D-NMR and MS) and literature comparison. Result: Seventeen compounds were isolated and identified as isolumichrome(1)

p-hydroxycinnamic acid(2)

benzoic acid(3)

p-hydroxy phenylethylamine(4)

p-hydroxy phenylethanol(5)

butylparaben(6)

adenosine(7)

3-[p-hydroxyphenyl]-propionic acid amide(8)

hetisine(9)

guanfu base H(10)

salidroside(11)

cyclo-(ile-leu)(12)

phenylalanine(13)

3-(4-aminophenyl)prop-2-enoic acid(14)

N-oxide hordenine(15)

(2R

3R)-2

4-trihydroxy-butanoic acid(16)

and N-methyltyramine(17). Conclusion: Compounds 1-4

6-8 and 12-17 were isolated from A. tanguticum for the first time.

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Related Author

LI Chun

LIN Li-mei

LI Zhong

HAN Yu

LIU Chang

LIU Jiao

ZHANG Tao

ZOU Zhongmei

Related Institution

Shenyang Pharmaceutical University

Institute of Medicinal Plant Development，Chinese Academy of Medical Sciences&Peking Union College

Henan University of Chinese Medicine

School of Food Science and Engineering，Guangdong Ocean University

School of Materials Science and Engineering，Guangdong Ocean University

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