Chemical Constituents of -butanol Fraction of Notoginseng Medicinal Fungal Substance (Ⅱ)

LIU Xiao-li; WANG Xin-wen; DING Cai-feng; QIU Zhi-dong; XU Wei

doi:10.13422/j.cnki.syfjx.2016070093

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Chemical Constituents of -butanol Fraction of Notoginseng Medicinal Fungal Substance (Ⅱ)

更新时间：2024-01-04

- Chemical Constituents of -butanol Fraction of Notoginseng Medicinal Fungal Substance (Ⅱ)
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 22, Issue 7, Pages: 93-95(2016)
- 作者机构：
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- DOI：10.13422/j.cnki.syfjx.2016070093
  CLC： R284
- Published：2016
- 稿件说明：
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LIU Xiao-li, WANG Xin-wen, DING Cai-feng, et al. Chemical Constituents of -butanol Fraction of Notoginseng Medicinal Fungal Substance (Ⅱ)[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(7): 93-95.
DOI：

LIU Xiao-li, WANG Xin-wen, DING Cai-feng, et al. Chemical Constituents of -butanol Fraction of Notoginseng Medicinal Fungal Substance (Ⅱ)[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(7): 93-95. DOI： 10.13422/j.cnki.syfjx.2016070093.

摘要

目的: 通过生物转化技术发酵三七获得三七药性菌质

对正丁醇部位化学成分进行研究。方法: 采用系统溶剂萃取、D101大孔吸附树脂、硅胶柱色谱、开放式ODS柱色谱、半制备液相色谱等方法进行分离纯化

结合化合物理化性质和波谱数据鉴定其化合物结构。结果: 从三七药性菌质正丁醇部位分离得到6个化合物

分别为24(R)-假人参皂苷RT5(1)

人参皂苷SG1(2)

人参皂苷Rh12(3)

人参皂苷Rb1(4)

vina-ginsenoside R8(5)

vina-ginsenoside R9(6)。结论: 化合物1

6为首次从三七植物中分离得到

所有化合物均为首次从三七药性菌质中分离得到。

Abstract

Objective: To investigate the chemical constituents of n-butanol fraction of notoginseng medicinal fungal substance which was obtained from notoginseng by biotransformation technology. Method: The compounds were isolated and purified through system solvent extraction

D101 macroporous adsorptive resin

silica gel column chromatography

open ODS column chromatography

and semi-preparative liquid chromatography. The structures of these isolated compounds were identified by means of chemical properties

spectroscopic analysis. Result: Six compounds were separated from n-butanol fraction of notoginseng medicinal fungal substance and identified as 24(R)-pseudoginsenoside RT5(1)

ginsenoside SG1(2)

ginsenoside Rh12(3)

ginsenoside Rb1(4)

vina-ginsenoside R8(5)

and vina-ginsenoside R9(6). Conclusion: Compounds 1

5 and 6 were isolated from this plant for the first time

and all compounds were isolated from notoginseng medicinal fungal substance for the first time.

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