LIANG Jin-liang, LIANG Yan, ZHOU Wei, et al. Determination of Organochlorine Pesticide Residues in Lonicerae Japonicae Flos by Different Pretreatment[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(10): 50-54.
DOI:
LIANG Jin-liang, LIANG Yan, ZHOU Wei, et al. Determination of Organochlorine Pesticide Residues in Lonicerae Japonicae Flos by Different Pretreatment[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(10): 50-54. DOI: 10.13422/j.cnki.syfjx.2016100050.
Determination of Organochlorine Pesticide Residues in Lonicerae Japonicae Flos by Different Pretreatment
Objective: To establish SPME-GC method for rapid determination of organochlorine pesticide residues (OCPs) in Lonicerae Japonicae Flos by comparing solid-phase microextraction (SPME) with other three pretreatment methods. Method: OCPs in Lonicerae Japonicae Flos were analyzed according to the methods in Chinese Pharmacopoeia 2010 edition
Japanese Pharmacopoeia 16th revision
Manual for China National Food Contamination and Harmful Factors Risk Monitoring in 2014 and solid phase microextraction technology (SPME)
and the recovery rates were calculated respectively. Result: Recovery rates of the four different pretreatment methods were determined between 65% to 120%. Among the methods
there was fewer impurity interference in Chinese Pharmacopoeia 2010 edition method
Japanese Pharmacopoeia 16th revision method and SPME. Conclusion: The effect of 4 methods on OCPs in Lonicerae Japonicae Flos was analyzed
Anti-inflammatory Effect and Mechanism of Active Constituents from Lonicerae Japonicae Flos and Lonicerae Flos: A Review
Quality Control of Dynamic Volatile Components in Lonicerae Japonicae Flos and Lonicerae Flos
Reaction of Chlorogenic Acid with Sulfite and Its Application in Identification of Sulfur-fumigated Herbs
Evaluation of HPLC Fingerprint of Lonicerae Japonicae Flos and Lonicerae Flos Based on Total Statistical Moment Analysis Method
Chemical Constituents and Pharmacological Effect of Lonicerae Japonicae Flos
Related Author
WEI Jingyue
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TUO Qinhui
YANG Dongmei
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