Influence of Sulfur-fumigation and Ventilation Baking on Contents of Atractylenolide Ⅰ and Ⅲ in Fresh Products of Atractylodis Macrocephalae Rhizoma

SUN Xue; WEN Hong-mei; LU Tu-lin; LI Wei; CUI Xiao-bing

doi:10.13422/j.cnki.syfjx.2016160010

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Influence of Sulfur-fumigation and Ventilation Baking on Contents of Atractylenolide Ⅰ and Ⅲ in Fresh Products of Atractylodis Macrocephalae Rhizoma

更新时间：2024-01-04

- Influence of Sulfur-fumigation and Ventilation Baking on Contents of Atractylenolide Ⅰ and Ⅲ in Fresh Products of Atractylodis Macrocephalae Rhizoma
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 22, Issue 16, Pages: 10-13(2016)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2016160010
  CLC： R283
- Published：2016
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SUN Xue, WEN Hong-mei, LU Tu-lin, et al. Influence of Sulfur-fumigation and Ventilation Baking on Contents of Atractylenolide Ⅰ and Ⅲ in Fresh Products of Atractylodis Macrocephalae Rhizoma[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(16): 10-13.
DOI：

SUN Xue, WEN Hong-mei, LU Tu-lin, et al. Influence of Sulfur-fumigation and Ventilation Baking on Contents of Atractylenolide Ⅰ and Ⅲ in Fresh Products of Atractylodis Macrocephalae Rhizoma[J]. Chinese journal of experimental traditional medical formulae, 2016, 22(16): 10-13. DOI： 10.13422/j.cnki.syfjx.2016160010.

摘要

目的：建立HPLC-PDA同时测定白术中白术内酯Ⅰ和白术内酯Ⅲ含量的方法，比较不同温度鼓风烘制与硫熏白术中这2种成分的含量，探究代替硫磺熏蒸的最佳温度鼓风烘制保存的加工方法。方法：不同温度鼓风烘制和硫磺熏蒸的白术提取物的分析采用Inertsil® ODS-SP色谱柱，流速1.0 mL·min-1，流动相乙腈-水（52：48），检测波长220 nm。结果：白术内酯Ⅰ和白术内酯Ⅲ的线性范围分别为20.4～326.4，20.9～334.4 ng（r>0.9995），加样回收率分别为99.43%和99.20%，RSD分别为0.2%和0.3%。70℃烘制的白术中白术内酯Ⅰ和白术内酯Ⅲ的含量最高。结论：高温鼓风烘制及硫磺熏蒸均会减少白术内酯Ⅰ和白术内酯Ⅲ的含量，建议采用70℃鼓风烘制法替代硫磺熏蒸作为白术的加工方法，该方法便捷、可靠、安全，为白术的质量控制提供参考。

Abstract

Objective: To establish a HPLC-PDA method for simultaneous determination of atractylenolide Ⅰ and Ⅲ in Atractylodis Macrocephalae Rhizoma

compare contents of these two constituents under sulfur-fumigation and ventilation baking

then explore a ventilation baking method to substitute sulfur-fumigation as the best processing method. Method: Analysis of Atractylodis Macrocephalae Rhizoma extract under sulfur-fumigation and ventilation baking was performed on Inertsil® ODS-SP column

mobile phase was acetonitrile-water (52:48)

flow rate was 1.0 mL·min-1

column temperature was maintained at 40℃ and chromatograms were monitored at 220 nm. Result: Good linear relationships of atractylenolide Ⅰ and Ⅲ were in the ranges of 20.4-326.4 ng and 20.9-334.4 ng with r>0.999 5

their average recoveries were 99.43% and 99.20% with RSD of 0.2% and 0.3%

respectively.Contents of atractylenolide Ⅰ and Ⅲ in Atractylodis Macrocephalae Rhizoma baked at 70℃ was the highest. Conclusion: High temperature baking and sulfur fumigation will reduce contents of atractylenolides

baking at 70℃ is the best processing method to substitute sulfur-fumigation for Atractylodis Macrocephalae Rhizoma.The method is convenient

reliable and safe.

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