Chemical Constituents of

GAO Yan-ping; WU Qiang; LIANG Jian; ZHONG Guo-yue

doi:10.13422/j.cnki.syfjx.2016180060

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Chemical Constituents of

更新时间：2024-01-04

- Chemical Constituents of
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 22, Issue 18, Pages: 60-63(2016)
- 作者机构：
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2016180060
  CLC： R29
- Published：2016
- 稿件说明：
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GAO Yan-ping, WU Qiang, LIANG Jian, et al. Chemical Constituents of [J]. Chinese journal of experimental traditional medical formulae, 2016, 22(18): 60-63.
DOI：

GAO Yan-ping, WU Qiang, LIANG Jian, et al. Chemical Constituents of [J]. Chinese journal of experimental traditional medical formulae, 2016, 22(18): 60-63. DOI： 10.13422/j.cnki.syfjx.2016180060.

摘要

目的：对矮紫堇的化学成分进行研究。方法：采用系统溶剂提取，通过反复硅胶柱色谱、凝胶Sephadex LH-20柱色谱、半制备高效液相色谱等技术进行分离纯化，运用NMR，MS等波谱方法以及结合文献数据对分离得到的化合物进行结构鉴定。结果：从藏族药矮紫堇中分离得到13个化合物，分别鉴定为芹菜素（1），槲皮素（2），木犀草素（3），山柰酚（4），5， 7， 4'-三羟基二氢黄酮（5），芦丁（6），槲皮苷（7），紫云英苷（8），乌苏酸（9），齐墩果酸（10），豆甾醇（11），β-谷甾醇（12），胡萝卜苷（13）。结论：所有化合物均为首次从该藏族药矮紫堇中分离得到。

Abstract

Objective: To investigate the chemical constituents of Corydalis hendersonii. Method: The constituents were extracted by using systematic solvents

separated and purified by repeated silica gel column chromatography

Sephadex LH-20 column chromatography

semi-preparative HPLC

etc. The structures of the obtained constituents were identified by using NMR

MS and other spectral methods as well as literature data. Result: Thirteen compounds were obtained and identified as apigenin(1)

quercetin(2)

luteolin(3)

kaempferol(4)

4'-trihydroxy flavanone(5)

rutin(6)

quercitrin(7)

astragalin(8)

ursolic acid(9)

oleanic acid(10)

stigmasterol(11)

β-sitosterol(12)

and daucosterol(13). Conclusion: All the components were obtained from Corydalis hendersonii for the first time.

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Related Institution

Dpartment of Chemistry,School of Chemistry and Chemical Engineering,Guizhou University

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