LIU Rong-hua, WANG Ding-qing, LIN Shuai, et al. Triterpenoids from Heartwood of [J]. Chinese journal of experimental traditional medical formulae, 2017, 23(20): 42-46.
DOI:
LIU Rong-hua, WANG Ding-qing, LIN Shuai, et al. Triterpenoids from Heartwood of [J]. Chinese journal of experimental traditional medical formulae, 2017, 23(20): 42-46. DOI: 10.13422/j.cnki.syfjx.2017200042.
Objective: To investigate the chemical constituents of triterpenoids in the heartwood of Dalbergia latifolia. Method: The heartwood samples of D.latifolia were crushed into powder and extracted with 70% ethanol for 3 times
2 h for each time.The filtrate liquid was collected and the solvent was decompressed and recovered to obtain extract.The extract was dispersed in water and then extracted successively with petroleum ester
dichloromethane
ethylacetate and butanol to obtain petroleum ester fraction
dichloromethane fraction
ethylacetate fraction and butanol fraction.The chemical compounds in the extract fractions were isolated by column chromatography technologies such as silica gel
Sephadex LH-20
reverse phase silica gel and macroporous resin
and the structures of the obtained monomeric compounds were identified through physical and chemical analysis
spectroscopic methods and mass spectrum analysis method. Result: Seven triterpenoids were isolated and identified as 3-O-α-L-arabinopyranosyl-28-O-β-D-glucopyranosyl pomolic acid (1)
β-sitostenone (2)
β-sitosterol (3)
stigmasterol (4)
β-amyrin acetate (5)
β-amyrin-3-palmitate (6)
and 3-acetoxy-oleanoic acid (7). Conclusion: Compounds 1
5
and 6 were isolated from Dalbergia genus for the first time.Compounds 2 and 4 were isolated from this plant for the first time.
Analysis of Chemical Constituents in Ethanol Extract of Cyclocarya paliurus Dried Leaves by UHPLC-Q-TOF/MS
Chemical Constituents of Ethyl Acetate Extract from Ajuga ovalifolia var. calantha
Rapid Analysis and Identification of Chemical Constituents from Siwei Tumuxiang San by HPLC-Q-Exactive-MS/MS
Isolation and Identification of Chemical Constituents from Ethanol Extract of Camptosorus sibiricus
Separation Identification of Chemical Constituents of Lysimachia capillipes
Related Author
Yan XIAO
Boji MA
Bingtao LI
Li JIANG
Rengeng SHU
Qiyun ZHANG
Guoliang XU
Tian-long YANG
Related Institution
Research Center for Differentiation and Development of Traditional Chinese Medicine (TCM) Basic Theory,Jiangxi Provincial Key Laboratory of TCM Etiopathogenisis,Key Laboratory of Pharmacology of TCM in Jiangxi,School of Pharmacy,Jiangxi University of Chinese Medicine
Key Laboratory of Standardization of Chinese Herbal Medicine,Ministry of Education,State Key Laboratory Breeding of Systematic Research Development and Utilization of Chinese Medical Resources, Co-founded by Sichuan Province and MOST,School of Pharmacy ,Chengdu University of Traditional Chinese Medicine
School of Pharmacy, Inner Mongolia Medical University
School of Clinical Medicine, Inner Mongolia Medical University
Shandong University of Traditional Chinese Medicine(TCM)