Chemical Constituents from

CAO Gui-yun; HUANG Jiao; ZHANG Qi-hang; LI Ke-ke; SHEN Li

doi:10.13422/j.cnki.syfjx.2017200047

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Chemical Constituents from

更新时间：2024-01-04

- Chemical Constituents from
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 23, Issue 20, Pages: 47-50(2017)
- 作者机构：
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- DOI：10.13422/j.cnki.syfjx.2017200047
  CLC： R284.1
- Published：2017
- 稿件说明：
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CAO Gui-yun, HUANG Jiao, ZHANG Qi-hang, et al. Chemical Constituents from [J]. Chinese journal of experimental traditional medical formulae, 2017, 23(20): 47-50.
DOI：

CAO Gui-yun, HUANG Jiao, ZHANG Qi-hang, et al. Chemical Constituents from [J]. Chinese journal of experimental traditional medical formulae, 2017, 23(20): 47-50. DOI： 10.13422/j.cnki.syfjx.2017200047.

摘要

目的：研究绒毛栗色鼠尾草（Salvia castanea）根的化学成分。方法：采用硅胶柱色谱，HPLC柱色谱等方法对绒毛栗色鼠尾草70%乙醇提取物的乙酸乙酯部位进行分离纯化，通过理化性质和波谱数据鉴定所得化合物的结构。结果：从绒毛栗色鼠尾草中分离出12个化合物，分别鉴定为正二十六烷（1），β-谷甾醇（2），3-O-乙酰基齐墩果醛（3），齐墩果酸（4），5，5'-二丁氧基-2，2'-双环呋喃（5），丁草胺（6），亚麻酸乙酯（7），咖啡酸乙酯（8），香草酸（9），原儿茶酸（10），原儿茶醛（11），5-羟甲基-2-呋喃甲醛（12）。结论：化合物 3， 5， 6 为首次从鼠尾草属植物中分离得到，化合物 1， 4， 7~10 和 12 为首次从该植物中分离得到。

Abstract

Objective: To study the chemical constituents from roots of Salvia castanea. Method: The ethyl acetate fraction of 70% ethanol extract of S.castanea was isolated and purified by silica gel column chromatographyand HPLC.Then their structures were elucidated by physicochemical properties and spectral data. Result: Twelve compounds were isolated and elucidated as n-hexacosane (1)

β-sitosterol (2)

3-O-acetyl oleanolic aldehyde (3)

oleanolic acid(4)

5'-dibutoxy-2

2'-bifuran(5)

butachlor(6)

ethyl linolenate(7)

caffeoyl ethyl ester (8)

vanillic acid (9)

protocatechuicacid (10)

protocatechualdehyde(11)

and 5-hydroxymethyl-2-furancarboxaldehyde(12). Conclusion: Compounds 3

and 6 were isolated from genus of Salvia for the first time; compounds 1

7-9 and 12 were first obtained from this plant.

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Related Institution

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