Determination Eugenol, Borneol and Isoborneol of Guanxin Shutong Capsule by Gas Chromatography

LIU Feng; MA Jiu-tai; SHAN Na; LU Xin-yi; DANG Yan-ni; YANG Dong-hua

doi:CNKI:11-3495/R.20110721.1734.008

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Determination Eugenol, Borneol and Isoborneol of Guanxin Shutong Capsule by Gas Chromatography

更新时间：2024-01-04

- Determination Eugenol, Borneol and Isoborneol of Guanxin Shutong Capsule by Gas Chromatography
- Chinese Journal of Experimental Traditional Medical Formulae Vol. 17, Issue 18, Pages: 56-59(2011)
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- DOI：CNKI:11-3495/R.20110721.1734.008
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- Published：2011
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LIU Feng, MA Jiu-tai, SHAN Na, et al. Determination Eugenol, Borneol and Isoborneol of Guanxin Shutong Capsule by Gas Chromatography[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(18): 56-59.
DOI：

LIU Feng, MA Jiu-tai, SHAN Na, et al. Determination Eugenol, Borneol and Isoborneol of Guanxin Shutong Capsule by Gas Chromatography[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(18): 56-59. DOI： CNKI:11-3495/R.20110721.1734.008.

摘要

目的: 建立同时测定冠心舒通胶囊中丁香酚、龙脑和异龙脑含量的气相色谱测定方法。方法: 采用气相色谱法

聚乙二醇20 000为固定相

涂布浓度为10 %

载气氮气

氢火焰离子化检测器。结果: 丁香酚在2.025 6~50.640 0 μg (r=0.999 5

n=6)

龙脑在29.90~104.65 μg (r=0.999 0

n=6)

异龙脑在30.2~105.7 μg(r=0.999 4

n=6)线性关系良好

平均加样回收率分别为100.95%

RSD 0.72%(n=6)

99.72%

RSD 0.38%(n=6)

100.47%

RSD 1.11%(n=6)。结论: 所建立的方法可同时对丁香酚、龙脑和异龙脑进行含量测定

准确、灵敏、重现性好

可用于冠心舒通胶囊的质量控制。

Abstract

Objective: The GC method was established for determination simulataneo of eugenol

borneol and isoborneol of Guanxin Shutong capsule. Method: The stationary phase of capillary column is polyethylene glycol 20 000

with 10% coating. Carrier gas is nitrogen

detector is Flame Ionization Detector(FID). Result: The standard curve was linear within the concentration range of 2.025 6-50.640 0 μg (r=0.999 0) for eugenol

29.9-104.65 μg (r=0.999 5)for borneol. and 30.2-105.7 μg(r=0.999 4) for isoborneol The average recovery of eugenol

borneol and isoborneol was 100.95%(n=6

RSD 0.72%)

99.72%(n=6

RSD 0.38%)and 100.47%(n=6

RSD 1.11%). Conclusion: The contents of eugenol

borneol and isoborneol in Guanxin Shutong capsule were determined in the first time. The method is simple

stability and feasible

controllable strong

which can be used to determinate the content of eugenol

borneol and isoborneol of Guanxin Shutong capsule.

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