4种不同基原郁金饮片水提液的石油醚提取部位GC-MS分析与比较

王雪梅; 石典花; 滕颖; 张学顺; 郝闪闪

doi:10.13422/j.cnki.syfjx.20180911

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4种不同基原郁金饮片水提液的石油醚提取部位GC-MS分析与比较

药剂与炮制 | 更新时间：2024-01-04

- 4种不同基原郁金饮片水提液的石油醚提取部位GC-MS分析与比较
- Analysis and Comparison of Petroleum Ether Extracts in Water Decoction of Curcumae Radix Pieces from Four Different Sources
- 中国实验方剂学杂志 2018年24卷第11期页码：9-15
- 作者机构：
- 作者简介：
- 基金信息：
  
  国家自然科学基金项目（81503255）;山东省中医药科技发展计划项目（2013-115）;国家中医药管理局中药炮制技术传承基地项目
- DOI：10.13422/j.cnki.syfjx.20180911
  中图分类号： R284.1
- 纸质出版：2018
- 稿件说明：
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王雪梅, 石典花, 滕颖, 等. 4种不同基原郁金饮片水提液的石油醚提取部位GC-MS分析与比较[J]. 中国实验方剂学杂志, 2018,24(11):9-15.

WANG Xue-mei, SHI Dian-hua, TENG Ying, et al. Analysis and Comparison of Petroleum Ether Extracts in Water Decoction of Curcumae Radix Pieces from Four Different Sources[J]. Chinese Journal of Experimental Traditional Medical Formulae, 2018, 24(11): 9-15.
王雪梅, 石典花, 滕颖, 等. 4种不同基原郁金饮片水提液的石油醚提取部位GC-MS分析与比较[J]. 中国实验方剂学杂志, 2018,24(11):9-15. DOI： 10.13422/j.cnki.syfjx.20180911.

WANG Xue-mei, SHI Dian-hua, TENG Ying, et al. Analysis and Comparison of Petroleum Ether Extracts in Water Decoction of Curcumae Radix Pieces from Four Different Sources[J]. Chinese Journal of Experimental Traditional Medical Formulae, 2018, 24(11): 9-15. DOI： 10.13422/j.cnki.syfjx.20180911.

摘要

目的：分析4种不同基原郁金饮片水提液的石油醚提取部位中化学成分，找出其共有成分及差异成分。方法：采用GC-MS对4种不同来源郁金饮片提取部位进行测定，载气为氦气，程序升温（从40℃开始，以4℃·min-1升到160℃，保持10 min；以2℃·min-1升到230℃，保持5 min），电离方式为电子轰击离子源。结果：从4种不同基原郁金饮片水提液的石油醚提取部位各分析出了50种成分，其中这4种饮片的共有成分有3种（香草醛，邻苯二甲酸二丁酯，棕榈酸），3种饮片的共有成分达9种，2种饮片共有成分达25种；4种饮片共有、交互存在的成分达37种，占检出成分总数的74%。结论：4种不同来源郁金饮片水提液的石油醚提取部位中存在共有和差异性成分，四者的共有及交互存在的成分应是其在临床作为同一药用的物质基础之一。

Abstract

Objective: To analyze the petroleum ether extracts in water decoction of Curcumae Radix pieces from four different sources

and find out the common and different components. Method: GC-MS was adopted to determine the petroleum ether extracts with carrier gas of helium

temperature was risen by program

ionization mode was electron bombardment ion source. Result: Fifty components were determined in the petroleum ether extracts in water decoction of Curcumae Radix pieces from four different sources

and 3 common components were found in four Curcumae Radix pieces;9 common components were found in three Curcumae Radix pieces;25 common components were found in two Curcumae Radix pieces;37 components were found in two or more Curcumae Radix pieces

accounting for 74% of total number of detected components. Conclusion: Curcumae Radix pieces from four different sources have common and different components in the petroleum ether extracts of water decoction

and the common and cross-existent components may be one of the material basis for using as the same medicine in the clinic.

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