HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量

查道成; 冯冬兰; 李林晓; 牛兰玲

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HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量

化学与分析 | 更新时间：2024-09-23

- HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量
- Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC
- 中国实验方剂学杂志 2013年19卷第9期页码：129-131
- 作者机构：
  
  1. 南阳医学高等专科学校
  2. 河南华茸堂药业有限公司
- 作者简介：
- 基金信息：
- DOI：
  中图分类号： R286
- 纸质出版日期：2013
- 稿件说明：
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[1]查道成,冯冬兰,李林晓,牛兰玲.HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量[J].中国实验方剂学杂志,2013,19(09):129-131.

ZHA Dao-cheng1, FENG Dong-lan1, LI Lin-xiao2, et al. Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 129-131.
[1]查道成,冯冬兰,李林晓,牛兰玲.HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量[J].中国实验方剂学杂志,2013,19(09):129-131. DOI：

ZHA Dao-cheng1, FENG Dong-lan1, LI Lin-xiao2, et al. Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 129-131. DOI：

摘要

目的:建立HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱含量测定方法。方法:色谱柱为大连依利特C18（4.6 mm×200 mm

5μm）

以乙腈-0.1%磷酸溶液（含0.1%三乙胺）（3∶97）为流动相

流速1 mL.min-1

检测波长205 nm

柱温30℃。结果:盐酸麻黄碱与样品中其他组分分离效果好

盐酸麻黄碱进样量在0.188～0.940μg具有良好线性关系

平均回收率99.39%

RSD 1.38%（n=6）。结论:方法简便易行

准确可靠

所建的方法可用于冯了性风湿跌打药酒的质量控制。

Abstract

Objective:To establish an HPLC method for determination of ephedrine hydrochloride in Fengliaoxing Fengshi Dieda wine.Method: The chromatographic column was Yilite C18（4.6 mm×200 mm

5 μm）;the mobile phase was acetonitril-0.1% phosphoric acid（0.1% triethameamine）（3∶ 97）;the flow rate was 1 mL · min-1;the detecting wavelength was set at 205 nm

and the column temperature was kept at 30 ℃.Result: The linear range of ephedrine hydrochloride was 0.188-0.940 μg.The average recovery was 99.39% and RSD was 1.38%（n=6）.Conclusion: The method established was accuracy

sensitive and simple.It can be used for quality control of Fengliaoxing Fengshi Dieda wine.

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