心脉康片的提取工艺优选

陈继英; 刘仔; 吴谋; 柯颖川

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心脉康片的提取工艺优选

工艺与制剂 | 更新时间：2024-09-23

- 心脉康片的提取工艺优选
- Optimization of Extraction Process of Xinmaikang Tablets by Orthogonal Test
- 中国实验方剂学杂志 2013年19卷第9期页码：59-61
- 作者机构：
  
  东莞市中医院
- 作者简介：
- 基金信息：
  
  东莞市科技计划医疗卫生类科研项目（201210515002013）
- DOI：
  中图分类号： R286;TQ461
- 纸质出版日期：2013
- 稿件说明：
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[1]陈继英,刘仔,吴谋,柯颖川.心脉康片的提取工艺优选[J].中国实验方剂学杂志,2013,19(09):59-61.

CHEN Ji-ying, LIU Zai, WU Mou, et al. Optimization of Extraction Process of Xinmaikang Tablets by Orthogonal Test[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 59-61.
[1]陈继英,刘仔,吴谋,柯颖川.心脉康片的提取工艺优选[J].中国实验方剂学杂志,2013,19(09):59-61. DOI：

CHEN Ji-ying, LIU Zai, WU Mou, et al. Optimization of Extraction Process of Xinmaikang Tablets by Orthogonal Test[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 59-61. DOI：

摘要

目的:优选心脉康片的提取工艺。方法:采用热循环回流提取浓缩机组方法

以干膏得率和辛弗林含量为指标

HPLC测定辛弗林含量

采用L9（34）正交试验对影响提取工艺的提取时间、加水量和蒸汽压进行考察。结果:心脉康片的最佳提取工艺为加15倍量水循环回流提取4 h

蒸汽压0.15 MPa。结论:该优选的提取工艺稳定、合理

可作为心脉康片的工业化生产提取工艺。

Abstract

Objective:To optimize water extraction technology of Xinmaikang tablets.Method: Heat circulating reflux extraction and concentration unit was taken

with yield of dry extract and the content of synephrine as indexes

the latter was determined by HPLC

effects of extraction time

the amount of water and vapor pressure on extraction technology of Xinmaikang tablets was investigated by orthogonal test.Result:Optimal extraction technology was as following:reflux extracted 4 h with 15 folds the amount of water

vapor pressure 0.15 MPa.Conclusion:This optimized extraction procedure was stable and reliable

and it could be used as industrial production extraction technology of Xinmaikang tablets.

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