MO Xiao-yu, MAI Jing-biao. Studies on Chemical Constituents of Chloroform Portion of [J]. Chinese journal of experimental traditional medical formulae, 2012, 18(23): 128-130.
MO Xiao-yu, MAI Jing-biao. Studies on Chemical Constituents of Chloroform Portion of [J]. Chinese journal of experimental traditional medical formulae, 2012, 18(23): 128-130.DOI:
13C-NMR)进行结构鉴定。 结果: 从三氯甲烷萃取部分分离5个化合物。分别鉴定为:evofolin B ( 1 )
ficusal ( 2 )
6-羟基-2-(4'-羟基-3'
5'-二甲氧基苯基)-3
7-二氧杂双环-[3.3.0]-辛烷 ( 3 )
N-反式阿魏酸酪酰胺( 4 )
lysicamine( 5 )。 结论: 上述化合物均为首次从该植物中分离得到。
Abstract
Objective: To study the chemical constituents of the chloroform portion of Incarvillea arguta. Method: The chloroform portion were isolated and pured by silica gel column chromatography
HP-20 and Sephadex LH-20.Their chemical structures were elucidated by spectral data(1H-NMR
13C-NMR). Result: Five compounds were isolated from the chloroform portion.They were identified as evofolin B( 1 )
ficusal( 2 )
6-hydroxy-2-(4'-hydroxy-3'
5'-dimethoxyphenyl)-3
7-dioxa-bicyclo-[3.3.0]-octane( 3 )
N-trans-feruloyl tyramine( 4 )
lysicamine( 5 ). Conclusion: All compounds were isolated from this plant for the first time.