顶空-气相色谱-质谱联用分析黄精炮制过程化学成分的变化

魏征; 曾林燕; 宋志前; 曹玉娜; 张琳琳; 刘振丽

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顶空-气相色谱-质谱联用分析黄精炮制过程化学成分的变化

更新时间：2024-01-04

- 顶空-气相色谱-质谱联用分析黄精炮制过程化学成分的变化
- Comparative Analysis of Chemical Constituent from Polygonati Rhizoma before and After Processing by Headspace Injection-GC-MS
- 中国实验方剂学杂志 2012年18卷第20期页码：115-118
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- 基金信息：
  
  国家自然科学基金面上课题(81073050)
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- 纸质出版日期：2012
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魏征, 曾林燕, 宋志前, 等. 顶空-气相色谱-质谱联用分析黄精炮制过程化学成分的变化[J]. 中国实验方剂学杂志, 2012,18(20):115-118.

WEI Zheng, ZENG Lin-yan, SONG Zhi-qian, et al. Comparative Analysis of Chemical Constituent from Polygonati Rhizoma before and After Processing by Headspace Injection-GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(20): 115-118.
魏征, 曾林燕, 宋志前, 等. 顶空-气相色谱-质谱联用分析黄精炮制过程化学成分的变化[J]. 中国实验方剂学杂志, 2012,18(20):115-118. DOI：

WEI Zheng, ZENG Lin-yan, SONG Zhi-qian, et al. Comparative Analysis of Chemical Constituent from Polygonati Rhizoma before and After Processing by Headspace Injection-GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(20): 115-118. DOI：

摘要

目的: 研究炮制前后黄精中化学成分的变化。方法: 制备不同炮制时间的酒黄精

顶空进样-气相色谱-质谱(GC-MS)联用技术进行分析

经数据库检索并参考正构烷烃标准品保留指数(RI)

确定化合物结构。应用色谱峰峰面积归一化法计算各成分的相对百分含量。结果: 生品与各炮制品共有的成分12个

但每种成分含量不同。与生品比较

炮制不同时间产生的成分20个

检测不到的成分7个。结论: 黄精炮制后化学成分组成和含量发生变化。

Abstract

Objective:To study the constituent changes of Polygonati Rhizoma before and after processing. Method: Polygonati Rhizoma was prepared with wine by stewing for different time. Headspace injection-GC-MS was used and the structures of compounds were identified by Data Base Retrieval and compared with the retention indexes of n-alkanes standards. The relative content of every constituent was obtained from the peak area normalization method of chromatographic peaks. Result: There are 12 common compounds between raw products and processed products

yet the relative content was different. Compared with raw products

20 compounds produced and 7 disappeared after different processed for different time. Conclusion: The chemical constituents and content have changed in the root of Polygonati Rhizoma before and after processing.

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