小儿清热止咳口服液澄清工艺比较

王玲; 周稚川; 高晓黎

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小儿清热止咳口服液澄清工艺比较

更新时间：2024-01-04

- 小儿清热止咳口服液澄清工艺比较
- Comparison of Clarification Technology for Xiao'er Qingre Zhike Oral Solution
- 中国实验方剂学杂志 2012年18卷第10期页码：55-59
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- 纸质出版日期：2012
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王玲, 周稚川, 高晓黎. 小儿清热止咳口服液澄清工艺比较[J]. 中国实验方剂学杂志, 2012,18(10):55-59.

WANG Ling, ZHOU Zhi-chuan, GAO Xiao-li. Comparison of Clarification Technology for Xiao'er Qingre Zhike Oral Solution[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(10): 55-59.
王玲, 周稚川, 高晓黎. 小儿清热止咳口服液澄清工艺比较[J]. 中国实验方剂学杂志, 2012,18(10):55-59. DOI：

WANG Ling, ZHOU Zhi-chuan, GAO Xiao-li. Comparison of Clarification Technology for Xiao'er Qingre Zhike Oral Solution[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(10): 55-59. DOI：

摘要

目的: 优选小儿清热止咳口服液的澄清工艺。方法: 比较高速离心法、乙醇沉淀法、ZTC1+1Ⅲ型天然澄清剂法3种澄清工艺对小儿清热止咳口服液中收膏率、麻黄碱和黄芩苷相对含量的影响。结果: 乙醇沉淀法为最佳澄清工艺

其工艺条件为药液浓度比1∶1

加95%乙醇调至含醇量60%

冷藏放置6 h。结论: 优选的澄清工艺稳定

可行。

Abstract

Objective: To optimize clarification technology of Xiao'er Qingre Zhike oral solution. Method: To compare effect of three clarification technology(high-speed centrifugation method

ethanol precipitation method and ZTC1+1Ⅲadsorption clarify agent method) on yield of extract and relative content of ephedrine and baicalin which were active components in Xiao'er Qingre Zhike oral solution. Result: The best clarification technology was ethanol precipitation method

its technology conditions were:the concentration ratio of sample liquid 1∶1 with adding 95% ethanol to adjust ethanol concentration to 60%

refrigerated 6 h. Conclusion: Optimized clarification technology for Xiao'er Qingre Zhike oral solution was stable and feasible.

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