均匀试验设计优选产妇康颗粒挥发油的包合工艺

贾永艳; 祝侠丽; 周红敏; 李九席; 魏超娟; 李翠萍; 田效志

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均匀试验设计优选产妇康颗粒挥发油的包合工艺

更新时间：2024-01-04

- 均匀试验设计优选产妇康颗粒挥发油的包合工艺
- Optimization of Inclusion Technology for Volatile Oil from Chanfukang Granule by Uniform Design
- 中国实验方剂学杂志 2012年18卷第12期页码：34-37
- 作者机构：
- 作者简介：
- 基金信息：
  
  郑州市科技攻关项目(064SGDS33221-3)
- DOI：
  中图分类号：
- 纸质出版日期：2012
- 稿件说明：
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贾永艳, 祝侠丽, 周红敏, 等. 均匀试验设计优选产妇康颗粒挥发油的包合工艺[J]. 中国实验方剂学杂志, 2012,18(12):34-37.

JIA Yong-yan, ZHU Xia-li, ZHOU Hong-min, et al. Optimization of Inclusion Technology for Volatile Oil from Chanfukang Granule by Uniform Design[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(12): 34-37.
贾永艳, 祝侠丽, 周红敏, 等. 均匀试验设计优选产妇康颗粒挥发油的包合工艺[J]. 中国实验方剂学杂志, 2012,18(12):34-37. DOI：

JIA Yong-yan, ZHU Xia-li, ZHOU Hong-min, et al. Optimization of Inclusion Technology for Volatile Oil from Chanfukang Granule by Uniform Design[J]. Chinese journal of experimental traditional medical formulae, 2012, 18(12): 34-37. DOI：

摘要

目的: 优化产妇康颗粒中挥发油的β-环糊精包合工艺。方法: 采用饱和水溶液法包合

以挥发油包合率为指标

以β-环糊精与挥发油的比例、包合温度、包合时间为考察因素

采用均匀试验优选包合工艺

并对包合物的物相进行验证。结果: 最佳工艺为挥发油与β-CD的比例1∶8

包合温度40 ℃

包合时间140 min。在该优选条件下

挥发油包合率达75%

验证结果显示包合物已形成。结论: 该优选的包合工艺合理、稳定、可行。

Abstract

Objective: To optimize inclusion process of volatile oil from Chanfukang granule. Method: Inclusion process was carried out by saturated aqueous solution method

inclusion process was optimized by uniform design with inclusion ratio of volatile oil as index

taking ratio of volatile oil to β-CD

inclusion temperature and inclusion time as factors

and physical phase of inclusion complex was verified. Result: Optimum inclusion process was as follows:ratio of volatile oil to β-CD 1∶8

inclusion temperature 40 ℃

inclusion time 140 min.Inclusion rate of volatile oil was as high as 75% under these optimized technology conditions.Validation result showed that inclusion compound had been formed. Conclusion: This optimized inclusion process was reasonable

stable and feasible.

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