毛冬青茎化学成分研究

应鸽; 丁平; 代蕾; 曹斯琼; 徐鸿华

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毛冬青茎化学成分研究

更新时间：2024-01-04

- 毛冬青茎化学成分研究
- Studies on Chemical Constituents of Stems of
- 中国实验方剂学杂志 2012年18卷第11期页码：118-120
- 作者机构：
- 作者简介：
- 基金信息：
  
  广东省重大科技专项(2008A030101009)
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  中图分类号：
- 纸质出版日期：2012
- 稿件说明：
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应鸽, 丁平, 代蕾, 等. 毛冬青茎化学成分研究[J]. 中国实验方剂学杂志, 2012,18(11):118-120.

YING Ge, DING Ping, DAI Lei, et al. Studies on Chemical Constituents of Stems of [J]. Chinese journal of experimental traditional medical formulae, 2012, 18(11): 118-120.
应鸽, 丁平, 代蕾, 等. 毛冬青茎化学成分研究[J]. 中国实验方剂学杂志, 2012,18(11):118-120. DOI：

YING Ge, DING Ping, DAI Lei, et al. Studies on Chemical Constituents of Stems of [J]. Chinese journal of experimental traditional medical formulae, 2012, 18(11): 118-120. DOI：

摘要

目的: 研究冬青科植物毛冬青茎的化学成分。方法: 通过硅胶柱色谱、SephadexLH-20柱色谱及反复重结晶等方法分离纯化化合物

利用核磁共振等现代波谱技术解析确定化合物结构。结果: 从毛冬青茎的石油醚和乙酸乙酯部位中分离并鉴定了5个化合物

分别为ilexgein A( 1 )

ilexsaponin A1( 2 )

ilexsaponin B1( 3 )

ilexsaponin B2( 4 )

β-谷甾醇( 5 )。结论: 化合物 1~5 均为首次从毛冬青茎中分离得到。

Abstract

Objective: To study the chemical constituents of the stems of Ilex pubescens. Method: The chemical constituents were isolated and purified via silica gel and Sephadex LH-20 column chromatography as well as recrystallization. Their structures were determined on the basis of spectral analysis and physicochemical properties. Result: Five compounds were isolated from the petroleum ether and EtOAc fractions.They were obtained and their structures were identified as ilexgein A( 1 )

ilexsaponin A1( 2 )

ilexsaponin B1( 3 )

Ilexsaponin B2( 4 )

β-sitosterol( 5 ). Conclusion: All of the five compounds were firstly isolated from the stems of I. pubescens.

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