固相微萃取-气相色谱-质谱联用分析贵州产杏叶茴芹挥发性成分

邢煜君; 常星; 张倩; 康文艺

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固相微萃取-气相色谱-质谱联用分析贵州产杏叶茴芹挥发性成分

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- 固相微萃取-气相色谱-质谱联用分析贵州产杏叶茴芹挥发性成分
- Analysis of Volatile Compounds from in Guizhou by SPME-GC-MS
- 中国实验方剂学杂志 2011年17卷第4期页码：93-95
- 作者机构：
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- 基金信息：
  
  河南省科技厅科技攻关重点项目(102102310019)
- DOI：
  中图分类号：
- 纸质出版日期：2011
- 稿件说明：
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邢煜君, 常星, 张倩, 等. 固相微萃取-气相色谱-质谱联用分析贵州产杏叶茴芹挥发性成分[J]. 中国实验方剂学杂志, 2011,17(4):93-95.

XING Yu-jun, CHANG Xing, ZHANG Qian, et al. Analysis of Volatile Compounds from in Guizhou by SPME-GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(4): 93-95.
邢煜君, 常星, 张倩, 等. 固相微萃取-气相色谱-质谱联用分析贵州产杏叶茴芹挥发性成分[J]. 中国实验方剂学杂志, 2011,17(4):93-95. DOI：

XING Yu-jun, CHANG Xing, ZHANG Qian, et al. Analysis of Volatile Compounds from in Guizhou by SPME-GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(4): 93-95. DOI：

摘要

目的: 研究贵州产杏叶茴芹挥发性成分。方法: 采用固相微萃取技术对杏叶茴芹挥发性成分进行提取

GC-MS进行鉴定。结果: 从杏叶茴芹挥发性成分中得到28个组分

鉴定了其中的19个化合物

占挥发性成分的86.23%。主要挥发性成分为(S)-1-甲基-4-(5-甲基-1-甲基-4-己烯基)环己烯 (48.83%) 和1-(1

5-二甲基-4-己烯基)-4-甲基苯 (6.15%)。结论 :杏叶茴芹挥发性成分主要是萜烯类。

Abstract

Objective: The volatile compounds from Pimpinella candolleana were studied. Method: Solid-phase micro-extraction (SPME) was used to extract the volatiles.The chemical constituents were analyzed by gas chromatography-mass spectrometry (GC-MS) coupled with Kovats index. Result: Twenty-eight compounds were separated and 19 compounds were identified

representative of 86.23% of total volatile compounds.The main compounds were (S)-1-methyl-4-(5-methyl-1-methylene-4-hexenyl)-cyclohexene (48.83%) and 1-(1

5-dimethyl-4-hexenyl)-4-methyl-benzene (6.15%). Conclusion: The main compounds in P.candolleana were terpenes.

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