三黄喷雾剂中黄芩、栀子提取物的大孔吸附树脂纯化工艺

朱鹏飞; 冯伟红; 刘淑芝

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三黄喷雾剂中黄芩、栀子提取物的大孔吸附树脂纯化工艺

更新时间：2024-01-04

- 三黄喷雾剂中黄芩、栀子提取物的大孔吸附树脂纯化工艺
- Purification Processes of Extract of Scutellaria and Gardenia from Sanhuang Spray with Macroporous Adsorption Resin
- 中国实验方剂学杂志 2010年16卷第17期页码：4-6
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- 基金信息：
  
  重大新药创制(2009ZX09502-010,2009ZX09301-005-05);中国中医科学院自主选题项目(Z02094)
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- 纸质出版日期：2010
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朱鹏飞, 冯伟红, 刘淑芝. 三黄喷雾剂中黄芩、栀子提取物的大孔吸附树脂纯化工艺[J]. 中国实验方剂学杂志, 2010,16(17):4-6.

ZHU Peng-fei, FENG Wei-hong, LIU Shu-zhi. Purification Processes of Extract of Scutellaria and Gardenia from Sanhuang Spray with Macroporous Adsorption Resin[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(17): 4-6.
朱鹏飞, 冯伟红, 刘淑芝. 三黄喷雾剂中黄芩、栀子提取物的大孔吸附树脂纯化工艺[J]. 中国实验方剂学杂志, 2010,16(17):4-6. DOI：

ZHU Peng-fei, FENG Wei-hong, LIU Shu-zhi. Purification Processes of Extract of Scutellaria and Gardenia from Sanhuang Spray with Macroporous Adsorption Resin[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(17): 4-6. DOI：

摘要

目的 :研究大孔吸附树脂纯化三黄喷雾剂中黄芩的工艺条件。方法 :采用HPLC测定黄芩苷含量

以黄芩苷的吸附率、解吸率为考察指标

优选大孔吸附树脂最佳纯化工艺条件。结果 :最佳大孔吸附树脂型号为SP-825;上样液浓度为0.2 g ·mL-1

径高比为1 ∶7

最大上样量为2 BV

洗脱剂为70%乙醇

洗脱流速为3 BV ·h-1

洗脱剂用量为6 BV。结论 :SP-825型大孔吸附树脂纯化黄芩、栀子提取物的最佳工艺稳定、可行。

Abstract

ObJective: To investigate the purification processes of Scutellaria from Sanhuang spray with macroporous adsorption resin. Method: The content of baicalin was measured with HPLC. The adsorption rate and desorption rate were measured to evaluate the optimal macroporous adsorption resin and the optimal purification conditions. Result: The optimal macroporous adsorption resin was SP-825. The optimal purification condition was as follows: the sample concentration was 0.2 g ·mL-1; the diameter height ratio was 1 ∶7; the sample volume was 2 BV; the eluant was 70% ethanol; the elution flow rate was 3 BV ·h-1; the ethanol consumption was 6 BV. Conclusion: Purification process of the extract of Scutellaria and Gardenia with SP-825 macroporous adsorption resin was stable and feasible.

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