闪式与回流提取黄芪皂苷工艺比较

赵强强; 韩丽; 熊永爱; 王淼; 谢兴亮; 杨明

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闪式与回流提取黄芪皂苷工艺比较

更新时间：2024-01-04

- 闪式与回流提取黄芪皂苷工艺比较
- Comparion of Smashing and Reflux Extraction Process for Astragaloside
- 中国实验方剂学杂志 2010年16卷第13期页码：1-3
- 作者机构：
- 作者简介：
- 基金信息：
  
  国家科技重大新药创制专项(2009ZX09103-307)
- DOI：
  中图分类号：
- 纸质出版日期：2010
- 稿件说明：
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赵强强, 韩丽, 熊永爱, 等. 闪式与回流提取黄芪皂苷工艺比较[J]. 中国实验方剂学杂志, 2010,16(13):1-3.

ZHAO Qiang-qiang, HAN Li, XIONG Yong-ai, et al. Comparion of Smashing and Reflux Extraction Process for Astragaloside[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(13): 1-3.
赵强强, 韩丽, 熊永爱, 等. 闪式与回流提取黄芪皂苷工艺比较[J]. 中国实验方剂学杂志, 2010,16(13):1-3. DOI：

ZHAO Qiang-qiang, HAN Li, XIONG Yong-ai, et al. Comparion of Smashing and Reflux Extraction Process for Astragaloside[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(13): 1-3. DOI：

摘要

目的 :考察闪式与回流提取对黄芪皂苷提取工艺的影响。方法 :以黄芪甲苷提取率和出膏率作为考察指标

采用HPLC-ELSD法作为测定方法

以Welc C18(4.6 mm×250 mm

5 μm)为色谱柱

乙腈:水(40 ∶60)为流动相

流速1 mL ·min-1

漂移管温度80 ℃

气流量50 psi

考察闪式与回流提取对黄芪皂苷提取工艺的影响。结果 :闪式提取所得黄芪甲苷含量高于回流提取。结论 :闪式提取黄芪皂苷不仅提取率高

而且耗时短

节省能源

可望广泛地应用在制药工业上。

Abstract

Objective: To study smashing and reflux extraction of astragaloside. Method: The extraction process was investigated by smashing and reflux extraction with the extraction of astragalosideⅣ and the rate of extracts as criteria. The measurement conditions were used as follows: Welc C18 (4.6 mm×250 mm

5 μm) column was used with acetonitrile:water (40 ∶60) as mobile phase; the flow rate was 1 mL ·min-1; the temperature of drift tube was set at 80 ℃; gas flow was 50 psi. Result: The conent of astragalosideⅣ of smashing extraction were higher than reflux extraction. Conclusion: Smashing extraction method for astragaloside can save time

working and energy

and it is hoped to be widely used in the pharmaceutical industry.

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