穴敷喘平凝胶贴剂质量标准研究

刘莉; 穆晓敏; 沈亦妙; 刘强

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穴敷喘平凝胶贴剂质量标准研究

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- 穴敷喘平凝胶贴剂质量标准研究
- Study on Quality Standards of Xuefu Chuanping Gel Patch
- 中国实验方剂学杂志 2010年16卷第11期页码：32-34
- 作者机构：
- 作者简介：
- 基金信息：
  
  国家自然科学基金项目(309973951);广东省科技计划项目(2007B031400007)
- DOI：
  中图分类号：
- 纸质出版日期：2010
- 稿件说明：
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刘莉, 穆晓敏, 沈亦妙, 等. 穴敷喘平凝胶贴剂质量标准研究[J]. 中国实验方剂学杂志, 2010,16(11):32-34.

LIU Li, MU Xiao-min, SHEN Yi-miao, et al. Study on Quality Standards of Xuefu Chuanping Gel Patch[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(11): 32-34.
刘莉, 穆晓敏, 沈亦妙, 等. 穴敷喘平凝胶贴剂质量标准研究[J]. 中国实验方剂学杂志, 2010,16(11):32-34. DOI：

LIU Li, MU Xiao-min, SHEN Yi-miao, et al. Study on Quality Standards of Xuefu Chuanping Gel Patch[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(11): 32-34. DOI：

摘要

目的: 建立穴敷喘平凝胶贴剂的质量标准。方法: 采用TLC法鉴别方中芥子、延胡索、细辛。采用HPLC法测定方中盐酸麻黄碱的含量。结果: 定性鉴别中检出芥子、延胡索、细辛

且分离度好、专属性强

阴性对照无干扰。HPLC测定盐酸麻黄碱在0.032～0.096 μg有较好的线性关系

平均回收率为98.12%

RSD为1.08%

凝胶贴剂中盐酸麻黄碱含量为4.25 mg ·g-1。结论: 所建立的质量控制方法准确、可靠、专属性强

可以用于该制剂的质量控制。

Abstract

Objective: To establish the quality standards of Xuefu Chuanping gel patch. Method: Semen Sinapis. Corydalis and Herba Asari were identified by thin layer chromatography(TLC). The content of ephedrina hydrochloridum was determined by high performance liquid chromatography(HPLC). Result: Semen Sinapis. Corydalis and Herba Asari were identified by thin layer chromatography(TLC). The characteristic identification was distinct and highly specific. Ephedrina hydrochloridum was linear in the range of 0.032～0.096 μg. Average recovery was 98.12%

RSD was 1.08%. The content of ephedrina hydrochloridum in gels was 4.25 mg ·g-1. Conclusion: The quality control method is reliable

accurate and specific. It can be used for quality control of Xuefu Chuanping gel patch.

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