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纸质出版日期:2010
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张金莲, 何敏, 谢一辉, 等. 正交法优选蜜麸炒樟帮枳壳炮制工艺[J]. 中国实验方剂学杂志, 2010,16(10):8-11.
ZHANG Jin-lian, HE Min, XIE Yi-hui, et al. Processing of Stir-frying with Honey Bran for Zhang-Ban Fructus Aurantii by Orthogonal Design[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(10): 8-11.
目的: 用正交试验法优选并确立樟帮枳壳蜜麸炒工艺
为规范蜜麸炒樟帮枳壳饮片的炮制工艺提供技术参数。 方法: 以柚皮苷含量、新橙皮苷含量、橙皮苷含量、色度差为指标
采用正交试验法对炮制温度
炮制时间
加麸量、加蜜量4因素
每个因素取4个水平
进行枳壳麸炒工艺优选考察。 结果: 炮制温度
炮制时间对实验结果均有显著影响
确定最佳枳壳麸炒工艺为:炮制温度200 ℃
炮制时间120 s
加麸量10%
加蜜量15%。 结论: 正交试验确定的最佳工艺合理、可靠、重复性好。
Objective: In order to regulate processing technology of stir-fried with honey bran for Zhang-Ban Fructus Aurantii to provide technical parameters
the orthogonal design was used to optimize and establish a technique of stir-fried with honey bran for Zhang-Ban Fructus Aurantii. Method: The orthogonal design with four factors (including temperature
time
bran amount and honey amout) and four levels was employed to determine the effects
and the contents of neohesperidin
naringin
hesperidin
and the color difference used as four indexes. Result: Temperature
time and bran amount had significant effects on experimental results. The processing technique of stir-frying with bran for Zhang-Ban Fructus Aurantii was that the amount of 10% bran and 15% honey were added and Zhang-Ban Fructus Aurantii was fried at 200 ℃ for 120 seconds. Conclusion: The optimum condition obtained through orthogonal experiments was reasonable
reliable and repeatable.
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