HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量

查道成; 冯冬兰; 李林晓; 牛兰玲

doi:10.11653/syfj2013090129

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HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量

更新时间：2024-09-23

- HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量
- Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC
- 中国实验方剂学杂志 2013年19卷第9期页码：129-131
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- DOI：10.11653/syfj2013090129
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- 纸质出版日期：2013
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查道成, 冯冬兰, 李林晓, 等. HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量[J]. 中国实验方剂学杂志, 2013,19(9):129-131.

ZHA Dao-cheng, FENG Dong-lan, LI Lin-xiao, et al. Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 129-131.
查道成, 冯冬兰, 李林晓, 等. HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱的含量[J]. 中国实验方剂学杂志, 2013,19(9):129-131. DOI： 10.11653/syfj2013090129.

ZHA Dao-cheng, FENG Dong-lan, LI Lin-xiao, et al. Determination of Ephedrine Hydrochloride in Fengliaoxing Fengshi Dieda Wine by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 129-131. DOI： 10.11653/syfj2013090129.

摘要

目的: 建立HPLC测定冯了性风湿跌打药酒中盐酸麻黄碱含量测定方法。方法: 色谱柱为大连依利特C18(4.6 mm×200 mm

5 μm)

以乙腈-0.1%磷酸溶液(含0.1%三乙胺)(3:97)为流动相

流速1 mL·min-1

检测波长205 nm

柱温30℃。结果: 盐酸麻黄碱与样品中其他组分分离效果好

盐酸麻黄碱进样量在0.188~0.940 μg具有良好线性关系

平均回收率99.39%

RSD 1.38%(n=6)。结论: 方法简便易行

准确可靠

所建的方法可用于冯了性风湿跌打药酒的质量控制。

Abstract

Objective: To establish an HPLC method for determination of ephedrine hydrochloride in Fengliaoxing Fengshi Dieda wine. Method: The chromatographic column was Yilite C18(4.6 mm×200 mm

5 μm); the mobile phase was acetonitril-0.1% phosphoric acid (0.1% triethameamine) (3: 97); the flow rate was 1 mL·min-1; the detecting wavelength was set at 205 nm

and the column temperature was kept at 30℃. Result: The linear range of ephedrine hydrochloride was 0.188-0.940 μg. The average recovery was 99.39% and RSD was 1.38% (n=6). Conclusion: The method established was accuracy

sensitive and simple. It can be used for quality control of Fengliaoxing Fengshi Dieda wine.

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