ZUO Ai-xue, MA Yun-shu, RAO Gao-xiong. Akaloids Roots of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(9): 136-139. DOI: 10.11653/syfj2013090136.
To provide the chemical data for resources development of Stephania mashanica
its chemical constituents were investigated; Method: The powered tuber of S. mashanica were extracted with 2% H2SO4-H2O and purified by silica gel
alumina oxide and Sephadex LH-20 column chromatograph. The structures were elucidated on the basis of spectral analysis and physico-chemical evidence. Result: Seven alkaloids were isolated from the thin sulfuric acid extracts of the fresh roots of Stephania mashanica
these alkaloids were identified as dicentrine (1)
(() -crebanine (2)
sinoacutine (3)
tetrahydrocolumbamine (4)
tetrahydropalmatine (5)
palmatine (6)
and jatrorrhizine (7). Conclusion: compounds 2-7 were obtained from this plant for the first time.