JI Lang, LIAO Qing, LV Wei, et al. Establishment of Rapid Determination Method for Residue of Sulfur Dioxide in Traditional Chinese Herbs[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(10): 66-69.
JI Lang, LIAO Qing, LV Wei, et al. Establishment of Rapid Determination Method for Residue of Sulfur Dioxide in Traditional Chinese Herbs[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(10): 66-69. DOI: 10.11653/syfj2013100066.
Objective: To establish a rapid method for determination of sulfur dioxide residue in Chinese herbal medicines. Method: By the principle of in dilute hydrochloric acid
the active metal zinc could restore the sulfurous acid or sulfite to produce hydrogen sulfide
while hydrogen sulfide could lead acetate test paper strips black.We had determined sulfur dioxide residue in 18 batches(3 categories
6 varieties) of Chinese herbal medicines
and then used the 'Chinese Pharmacopoeia' method to verify this experimental method. Result: PbS spots of each batch of Chinese herbal medicines was clear
then compared with standard color card
you could determine the range of sulfur dioxide residue. Conclusion: This method was simple with short measurement time and simple device
it could be applied to rapid qualitative or semiquantitative determination of sulfur dioxide residues in Chinese herbal medicines.