HPLC鉴别哮喘宁片中五味子与南五味子

张汶婕; 杨惠; 万庆; 陈叶平

doi:10.11653/syfj2013100153

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HPLC鉴别哮喘宁片中五味子与南五味子

更新时间：2024-01-04

- HPLC鉴别哮喘宁片中五味子与南五味子
- Identification of Fructus Schisandra chinensis and Fructus Schisandra Sphenanthera in Xiaochuanning Tablets by HPLC
- 中国实验方剂学杂志 2013年19卷第10期页码：153-155
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- DOI：10.11653/syfj2013100153
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- 纸质出版日期：2013
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张汶婕, 杨惠, 万庆, 等. HPLC鉴别哮喘宁片中五味子与南五味子[J]. 中国实验方剂学杂志, 2013,19(10):153-155.

ZHANG Wen-jie, YANG Hui, WAN Qing, et al. Identification of Fructus Schisandra chinensis and Fructus Schisandra Sphenanthera in Xiaochuanning Tablets by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(10): 153-155.
张汶婕, 杨惠, 万庆, 等. HPLC鉴别哮喘宁片中五味子与南五味子[J]. 中国实验方剂学杂志, 2013,19(10):153-155. DOI： 10.11653/syfj2013100153.

ZHANG Wen-jie, YANG Hui, WAN Qing, et al. Identification of Fructus Schisandra chinensis and Fructus Schisandra Sphenanthera in Xiaochuanning Tablets by HPLC[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(10): 153-155. DOI： 10.11653/syfj2013100153.

摘要

目的: 鉴别哮喘宁片中五味子与南五味子。方法: 以五味子酯甲、五味子醇甲、五味子甲素、五味子乙素为对照

采用SunFireTM C18柱(4.6 mm×150 mm

5μm)

乙腈-四氢呋喃-水梯度洗脱

检测波长254 nm

流速1.0 mL·min-1

用中国药典委员会颁布的中药色谱指纹图谱相似度评价系统软件(2004A)进行相似度的比较。结果: 五味子药材及其成药制剂、南五味子药材及其成药制剂指纹图谱相似度均<0.9

但五味子、南五味子指纹图谱相似度<0.2。结论: 采用色谱技术能够鉴别哮喘宁片中五味子与南五味子。

Abstract

Objective: To identify Fructus Schisandra chinensis and Fructus Schisandra Sphenanthera in Xiaochuanning Tablets. Method: Schisantherin A

schisandrin

deoxyschizandrin

schizandrin B served as the reference substances. The assay was conducted on SunFireTM C18 column (4.6 mm×150 mm

5 μm) with acetonitrile-tetrahydrofuran-water as mobile phase. The flow rate was 1.0 mL·min-1 and the detection wavelength was set at 254 nm. Similarity evaluation system for chromatographic fingerprint of TCM (2004 A) was used in data analysis. Result: Fructus Schisandra Chinensis from habitats were of strong similarity with those from Xiaochuanning Tablets

but the similarities with Fructus Schisandra Sphenanthera from habitats or tablets were less than 0.20. Conclusion: HPLC can be used for identification of Fructus Schisandra Chinensis and Fructus Schisandra Sphenanthera in Xiaochuanning Tablets.

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