不同大孔树脂富集山茱萸中环烯醚萜苷的效果比较

蔡黎明; 周盈; 蔡宝昌; 刘芳; 皮文霞

doi:10.11653/syfj2013130039

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不同大孔树脂富集山茱萸中环烯醚萜苷的效果比较

更新时间：2024-01-04

- 不同大孔树脂富集山茱萸中环烯醚萜苷的效果比较
- Comparison of Enrichment Effect of Iridoid Glycosides from by Different Macroporous Resins
- 中国实验方剂学杂志 2013年19卷第13期页码：39-41
- 作者机构：
- 作者简介：
- 基金信息：
  
  国家自然科学基金项目(81274056)
- DOI：10.11653/syfj2013130039
  中图分类号：
- 纸质出版日期：2013
- 稿件说明：
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蔡黎明, 周盈, 蔡宝昌, 等. 不同大孔树脂富集山茱萸中环烯醚萜苷的效果比较[J]. 中国实验方剂学杂志, 2013,19(13):39-41.

CAI Li-ming, ZHOU Ying, CAI Bao-chang, et al. Comparison of Enrichment Effect of Iridoid Glycosides from by Different Macroporous Resins[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(13): 39-41.
蔡黎明, 周盈, 蔡宝昌, 等. 不同大孔树脂富集山茱萸中环烯醚萜苷的效果比较[J]. 中国实验方剂学杂志, 2013,19(13):39-41. DOI： 10.11653/syfj2013130039.

CAI Li-ming, ZHOU Ying, CAI Bao-chang, et al. Comparison of Enrichment Effect of Iridoid Glycosides from by Different Macroporous Resins[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(13): 39-41. DOI： 10.11653/syfj2013130039.

摘要

目的: 考察不同类型大孔树脂对山茱萸中环烯醚萜苷类成分的分离效果。方法: 采用HPLC测定山茱萸中马钱苷及莫诺苷的含量

考察不同大孔吸附树脂分离山茱萸中环烯醚萜苷类成分的有效性。结果: 马钱苷、莫诺苷的回归方程依次为Y=17.245X+13.362(r=0.999 9)

Y=15.468X-41.275(r=1.000 0);线性范围分别为21.75~435

35.8~716 μg;加样回收率分别为98.27%

96.29%。HPD-400型大孔树脂的分离效果最好。结论: 选取马钱苷和莫诺苷含量为指标筛选富集环烯醚萜苷的大孔树脂类型是可行的

研究结果为分离山茱萸中有效部位的后续研究提供实验依据。

Abstract

Objective:To investigate separation effect of iridoid glycosides from Cornus officinalis by different types of macroporous resin. Method: The content of loganin and morroniside from C. officinalis was determined by HPLC

effectiveness of different macroporous adsorption resin on separating iridoid glycosides from C. officinalis was investigated. Result: HPD-400 type of macroporous resin had the best separation effect.Regression equation of loganin and morroniside were Y=17.245X+13.362(r=0.999 9)

Y=15.468X-41.275(r=1.000 0);The linear range of them were 21.75-435

35.8-716 μg;Recoveries were 98.27%

96.29%

respectively. Conclusion: It was feasible that selected the content of loganin and morroniside as index to screen macroporous resin for enrichment iridoid glycosides from C. officinalis

this study could provide experimental basis for the follow-up study of separation of effective parts from C. officinalis.

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