
浏览全部资源
扫码关注微信
纸质出版日期:2013
移动端阅览
何俏明, 覃洁萍, 黄艳, 等. 草果果仁及果壳挥发油化学成分的GC-MS分析[J]. 中国实验方剂学杂志, 2013,19(14):112-117.
HE Qiao-ming, QIN Jie-ping, HUANG Yan, et al. Analysis of Volatile Oils from the Seeds and Shells of by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(14): 112-117.
何俏明, 覃洁萍, 黄艳, 等. 草果果仁及果壳挥发油化学成分的GC-MS分析[J]. 中国实验方剂学杂志, 2013,19(14):112-117. DOI: 10.11653/syfj2013140112.
HE Qiao-ming, QIN Jie-ping, HUANG Yan, et al. Analysis of Volatile Oils from the Seeds and Shells of by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(14): 112-117. DOI: 10.11653/syfj2013140112.
目的: 分析草果果仁、果壳挥发油的化学成分的差异
为其开发及应用提供基础。 方法: 采用水蒸气蒸馏法分别提取草果果仁及果壳的挥发油
并计算其含量;用气相色谱-质谱联用(GC-MS)法分析鉴定各挥发油的化学成分组成及结构。 结果: 从3个不同批次的草果中共鉴定出75个成分。其中从草果仁挥发油样品中分别鉴定出35
48
42个组分
分别占挥发油总量的94.8%
95.6%
93.7%;从果壳挥发油中分别鉴定出55
70
68个组分
分别占其挥发油总量的94.5%
91.5%
91.4%。其中果仁挥发油共有成分有33个
果壳挥发油共有成分有54个;果壳与果仁挥发油成分大部分相同
其共有成分主要有1
8-桉油素、α-蒎烯、β-蒎烯、α-松油醇、橙花叔醇等29个成分
分别占果壳和果仁挥发油总成分的69.27%~77.29%
91.56%~93.88%。草果果壳挥发油的特有成分有β-桉叶醇、葑醇、反式-松香芹醇、δ-杜松烯、(-)-桃金娘烯醇等18个化合物
果仁挥发油中无此类成分。 结论: 草果果壳挥发油含量约为果仁的1/4
果壳及果仁的挥发油成分大部分相同
均含有较高含量的1
8-桉油素和α-松油醇
但两者成分仍存在一定差异。
Objective: To analyze the chemical constituents of volatile oil from the seeds and shells of Amomum taso-Ko
and provide a basis for its development and application. Method: The steam distillation was used to the extraction of volatile oils and then calculated its content. The constituents of these volatile oils were separated and identified by GC-MS. Result: 35
48
42 compounds of three volatile oils of Amomum tsao-ko seeds from different origins were identified respectively
which account for 94.8%
95.6%
93.7% of their total peak area respectively. 55
70
68 compounds of the volatile oil samples from Amomum tsao-ko shells were identified
which account for 94.5%
91.5%
91.4% of their total oils. There were 29 common constituents in the volatile oil from the seeds and shells of Amomum taso-ko
which were 1
8-cineole
α-pinene
β-pinene
α-terpineol
nerolidol
and so on
which account for 95.4%-94.1% and 71.0%-77.6% of the total oils from the seeds and shells respectively. There were 18 special constituents in the volatile oils from the shells of Amomum taso-ko
such as β-eudesmol
fenchol
trans-(-)pinocarveol
δ-cadinene
(-)-myrtenol
and so on
which were not be found in the volatile oils from the seeds. Conclusion: The volatile oils from the shells were about 1/4 of the seeds'. Most of the constituents in the volatile oils from the seeds and shells of Amomum taso-ko are similar
all of the volatile oils contain a higher content of 1
8-cineole and α-terpineol
but still have some difference between the constituents of these two kinds of volatile oils.
0
浏览量
7
下载量
0
CSCD
关联资源
相关文章
相关作者
相关机构
京公网安备11010802024621