电导率法在线监测栀子提取物大孔树脂柱分离工艺

张鹏; 高峻峰; 孟硕; 刘建勋

doi:10.11653/syfj2013150027

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电导率法在线监测栀子提取物大孔树脂柱分离工艺

更新时间：2024-01-04

- 电导率法在线监测栀子提取物大孔树脂柱分离工艺
- Online Monitoring of Separation Technology with Macroporous Resin Column for Extract of by Conductivity Method
- 中国实验方剂学杂志 2013年19卷第15期页码：27-28
- 作者机构：
- 作者简介：
- 基金信息：
  
  国家自然科学基金项目(30772755,81073060);国家科技重大专项(2009ZX09103-317)
- DOI：10.11653/syfj2013150027
  中图分类号：
- 纸质出版日期：2013
- 稿件说明：
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张鹏, 高峻峰, 孟硕, 等. 电导率法在线监测栀子提取物大孔树脂柱分离工艺[J]. 中国实验方剂学杂志, 2013,19(15):27-28.

ZHANG Peng, GAO Jun-feng, MENG Shuo, et al. Online Monitoring of Separation Technology with Macroporous Resin Column for Extract of by Conductivity Method[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(15): 27-28.
张鹏, 高峻峰, 孟硕, 等. 电导率法在线监测栀子提取物大孔树脂柱分离工艺[J]. 中国实验方剂学杂志, 2013,19(15):27-28. DOI： 10.11653/syfj2013150027.

ZHANG Peng, GAO Jun-feng, MENG Shuo, et al. Online Monitoring of Separation Technology with Macroporous Resin Column for Extract of by Conductivity Method[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(15): 27-28. DOI： 10.11653/syfj2013150027.

摘要

目的: 利用电导法在线监测栀子提取液大孔树脂柱分离工艺。方法: 利用电导计测定通过大孔树脂柱洗脱后流出成分的电导率变化

并考察其与去乙酰基车叶草苷酸甲酯、京尼平-1-β-D龙胆双糖苷、栀子苷3个成分变化的相关性。结果: 电导率先下降

之后随栀子等成分的被洗脱又明显升高

呈较好的相关性。结论: 电导法可用于监测栀子提取物的大孔树脂分离工艺。

Abstract

Objective: To investigate online monitoring of separation technology with macroporous resin column for extract of Gardenia jasminoides by conductivity method. Method: Conductivity changes of eluted components after macroporous resin absorption were determined by conductivity apparatus

and its correlation with changes of geniposide

genipin-1-β-D-gentiobioside and deacetyl-asperulosidic acid methyl ester was detremined respectively. Result: Conductivity decreased first

and then significantly increased with elution of geniposide and other components

showing a good correlation. Conclusion: Conductance method could be used to monitor separation technology with macroporous resin for extract of G. jasminoides.

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