不同产地白豆蔻挥发油成分的GC-MS分析

冯旭; 梁臣艳; 牛晋英; 郭蕊; 张玄薇

doi:10.11653/syfj2013160107

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不同产地白豆蔻挥发油成分的GC-MS分析

更新时间：2024-01-04

- 不同产地白豆蔻挥发油成分的GC-MS分析
- Analysis of Volatile Constituents in from Various Habitats by GC-MS
- 中国实验方剂学杂志 2013年19卷第16期页码：107-110
- 作者机构：
- 作者简介：
- 基金信息：
  
  广西自然科学基金项目(2011GXNSFF018006)
- DOI：10.11653/syfj2013160107
  中图分类号：
- 纸质出版日期：2013
- 稿件说明：
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冯旭, 梁臣艳, 牛晋英, 等. 不同产地白豆蔻挥发油成分的GC-MS分析[J]. 中国实验方剂学杂志, 2013,19(16):107-110.

FENG Xu, LIANG Chen-yan, NIU Jin-ying, et al. Analysis of Volatile Constituents in from Various Habitats by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(16): 107-110.
冯旭, 梁臣艳, 牛晋英, 等. 不同产地白豆蔻挥发油成分的GC-MS分析[J]. 中国实验方剂学杂志, 2013,19(16):107-110. DOI： 10.11653/syfj2013160107.

FENG Xu, LIANG Chen-yan, NIU Jin-ying, et al. Analysis of Volatile Constituents in from Various Habitats by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(16): 107-110. DOI： 10.11653/syfj2013160107.

摘要

目的: 分析与比较不同产地白豆蔻挥发油的化学成分。方法: 采用HP-5MS弹性石英毛细管柱

程序升温

以EI离子源和四极杆质量分析器进行分析

质谱图用NIST08和Wiley275谱库检索

鉴定各种成分

并用色谱峰面积归一化法测定其相对百分含量。结果: 不同产地的白豆蔻挥发油中均含有桉油精、α-律草烯、β-蒎烯、α-蒎烯、α-荜澄茄烯、百里香素等19个化合物

但含量不同。结论: 不同产地白豆蔻挥发油的主要成分存在差异。

Abstract

Objective: To analyze the constituents of volatile oils in Amomum kravanh from various habitats. Method: The column temperature was controlled by a program with capillary column HP-5MS and the MS analysis was performed with EI and quadruple mass analyzer. The chemical composition was identified by NIST08 and Wiley275 library

and their relative contents were determined by using normalization method of chromatographic peak areas. Result: There were 19 common compounds in A. kravanh from various habitats which were eucalyptol

α-caryophyllene

β-pinene

α-pinene

α-cubebene

o-cymene. Conclusion: The main constituents were different in various habitats.

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