调经种玉丸定性定量研究

钱芳; 刘志辉; 陆超

doi:10.11653/syfj2013170139

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调经种玉丸定性定量研究

更新时间：2024-01-04

- 调经种玉丸定性定量研究
- Qualitative and Quantitative Analysis on Tiaojing Zhongyu Pills
- 中国实验方剂学杂志 2013年19卷第17期页码：139-142
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- DOI：10.11653/syfj2013170139
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- 纸质出版日期：2013
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钱芳, 刘志辉, 陆超. 调经种玉丸定性定量研究[J]. 中国实验方剂学杂志, 2013,19(17):139-142.

QIAN Fang, LIU Zhi-hui, LU Chao. Qualitative and Quantitative Analysis on Tiaojing Zhongyu Pills[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(17): 139-142.
钱芳, 刘志辉, 陆超. 调经种玉丸定性定量研究[J]. 中国实验方剂学杂志, 2013,19(17):139-142. DOI： 10.11653/syfj2013170139.

QIAN Fang, LIU Zhi-hui, LU Chao. Qualitative and Quantitative Analysis on Tiaojing Zhongyu Pills[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(17): 139-142. DOI： 10.11653/syfj2013170139.

摘要

目的: 制定调经种玉丸的定性定量控制方法。方法: 用薄层色谱法对制剂中川芎、丹参、续断、熟地进行定性鉴别;用高效液相色谱法对制剂中阿魏酸进行含量测定。结果: 各薄层定性鉴别色谱中

所鉴别的药材薄层色谱特征明显

在与对照药材或对照品相应的位置上显相同颜色的斑点

阴性无干扰。阿魏酸在4.68~62.34 ng呈良好的线性关系

Abstract

Objective: To find a better analytic method to determine Tiaojing Zhongyu Pills qualitatively and quantitatively. Method: Rhizoma Chuanxiong

Radix Salviae Miltiorrhizae

Radix Dipsali

Radix Rehmanniae Praeparata were identified by TLC. A method of HPLC to determine content of ferulic acid in the preparation was developed. Result: The studies on the quality control showed that the characteristics for identification by TLC were distinct. The quantification method had the linear range of 4.68-62.34 ng (r=1.000 0). The average recovery was 99.89% (RSD 0.79%). Conclusion: The method can be used as a quality control standard of Tiaojing Zhongyu Pills.

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