YU Ming-jie, CHEN Qing-zhu, DAI Qing, et al. Quality Standard of Ziyin Shengfa Granules[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(17): 143-145.
YU Ming-jie, CHEN Qing-zhu, DAI Qing, et al. Quality Standard of Ziyin Shengfa Granules[J]. Chinese journal of experimental traditional medical formulae, 2013, 19(17): 143-145. DOI: 10.11653/syfj2013170143.
Objective: To establish the quality standard for Ziyinshengfa Granules. Method: The thin-layer chromatograph (TLC) method was used to identify Radix Polygoni Multiflori Preparata
Fructus Lycii
Radix Salviae Miltiorrhizae and the content of 2
3
4
5'-tetahyd roxy stilbence-2-O-β-D-glucoside was determined by RP-HPLC. Result: The characteristic spots of Radix Polygoni Multiflori Preparata
Fructus Lycii
Radix Salviae Miltiorrhizae appeared in the TLC
and there was no interference for the negative sample. The linear range of 2
3
4
5'-tetahyd roxy stilbence-2-O-β-D-glucoside was 0.190 5-1.143 2 mg·L-1 (r=0.999 9). The average recovery rates were 98.60% (RSD 2.28%) (n=9). Conclusion: This method is simple
rapid
precise and reproducible
thus it can be used for the quality control of Ziyinshengfa Granules.