独一味环烯醚萜苷胶囊质量标准研究

尉丽力; 邱建国; 李茂星; 张泉龙; 周珺; 贾正平

doi:10.11653/syfj2013220137

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独一味环烯醚萜苷胶囊质量标准研究

更新时间：2024-01-04

- 独一味环烯醚萜苷胶囊质量标准研究
- Quality Standard of Iridoid Glycosides Capsule of
- 中国实验方剂学杂志 2013年19卷第22期页码：137-140
- 作者机构：
- 作者简介：
- 基金信息：
  
  甘肃省科技重大专项(1102FKDA012)
- DOI：10.11653/syfj2013220137
  中图分类号：
- 纸质出版日期：2013
- 稿件说明：
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尉丽力, 邱建国, 李茂星, 等. 独一味环烯醚萜苷胶囊质量标准研究[J]. 中国实验方剂学杂志, 2013,19(22):137-140.

WEI Li-li, QIU Jian-guo, LI Mao-xing, et al. Quality Standard of Iridoid Glycosides Capsule of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(22): 137-140.
尉丽力, 邱建国, 李茂星, 等. 独一味环烯醚萜苷胶囊质量标准研究[J]. 中国实验方剂学杂志, 2013,19(22):137-140. DOI： 10.11653/syfj2013220137.

WEI Li-li, QIU Jian-guo, LI Mao-xing, et al. Quality Standard of Iridoid Glycosides Capsule of [J]. Chinese journal of experimental traditional medical formulae, 2013, 19(22): 137-140. DOI： 10.11653/syfj2013220137.

摘要

目的: 制定独一味环烯醚萜苷胶囊的质量标准。方法: 以薄层色谱法对本品主成分进行定性鉴别

采用一阶导数法测定总环烯醚萜苷含量

高效液相色谱法测定山栀苷甲酯、8-O-乙酰山栀苷甲酯的含量。结果: 薄层色谱法样品与对照品在相同位置斑点清晰;一阶导数分光光度法测得3批总环烯醚萜苷含量均>50%;山栀苷甲酯、8-O-乙酰山栀苷甲酯与其他组分基线分离且峰形较好

测得3批样品平均含量为73.96

72.43 mg·g-1。结论: 该方法可以用于独一味环烯醚萜苷胶囊的质量控制。

Abstract

Objective: To establish the quality standard of iridoid glycosides capsule of Lamiophlomis rotata (IGC). Method: The iridoid glycosides capsule of L. rotata was identified by TLC. The contents of total iridoid glycosides

shanzhiside methyl ester and 8-O-acetylshanzhiside methyl ester in the capsule were determined by the first derivating UV-spectra and HPLC. Result: The identify spots were clear in TLC

and the constituents were well separated under the chromatographic condition. The contents of total iridoid glycosides of three batch capsule were more than 50%

the shanzhiside methyl ester and 8-O-acetylshanzhiside methyl ester were separated with other composition and the content were 73.96

72.43 mg·g-1 respectively. Conclusion: The method can be used to control the quality of IGC.

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