气相色谱-质谱联用技术研究半夏厚朴汤配伍对挥发油成分的影响

徐群; 武露凌; 王彩萍; 汪水娟; 孔令东

doi:10.13422/j.cnki.syfjx.2009.02.004

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气相色谱-质谱联用技术研究半夏厚朴汤配伍对挥发油成分的影响

质量标准 | 更新时间：2024-09-23

- 气相色谱-质谱联用技术研究半夏厚朴汤配伍对挥发油成分的影响
- Effects of Different Compatibility of Banxiahoupu Decoction on Changes of Volatile Oils by GC-MS
- 中国实验方剂学杂志 2009年15卷第2期页码：5-10
- 作者机构：
  
  1. 南京大学医药生物技术国家重点实验室
  2. 江苏省体育科学研究所
- 作者简介：
- 基金信息：
  
  国家自然科学基金重大研究计划中医药学几个关键问题的现代研究项目（90409009）
- DOI：10.13422/j.cnki.syfjx.2009.02.004
  中图分类号： R284.1
- 纸质出版日期：2009
- 稿件说明：
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[1]徐群,武露凌,王彩萍,汪水娟,孔令东.气相色谱-质谱联用技术研究半夏厚朴汤配伍对挥发油成分的影响[J].中国实验方剂学杂志,2009,15(02):5-10.

XU Qun~1, WU Lu-ling~2, WANG Cai-ping~1, et al. Effects of Different Compatibility of Banxiahoupu Decoction on Changes of Volatile Oils by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(2): 5-10.
[1]徐群,武露凌,王彩萍,汪水娟,孔令东.气相色谱-质谱联用技术研究半夏厚朴汤配伍对挥发油成分的影响[J].中国实验方剂学杂志,2009,15(02):5-10. DOI： 10.13422/j.cnki.syfjx.2009.02.004.

XU Qun~1, WU Lu-ling~2, WANG Cai-ping~1, et al. Effects of Different Compatibility of Banxiahoupu Decoction on Changes of Volatile Oils by GC-MS[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(2): 5-10. DOI： 10.13422/j.cnki.syfjx.2009.02.004.

摘要

目的:分析半夏厚朴汤及相关配伍样品挥发油成分种类和相对含量等变化

探讨半夏厚朴汤配伍与其挥发油成分变化的关系及规律。方法:利用气相色谱-质谱（GC-MS）法分离检测复方半夏厚朴汤、单味药厚朴、紫苏叶、生姜、及厚朴与紫苏叶、厚朴与生姜、紫苏叶与生姜等配伍样品挥发油成分。结果:各样品具有数目不同的挥发性成分

其中半夏厚朴汤54个、厚朴44个、紫苏叶15个、生姜53个、及配伍厚朴与紫苏叶26个、厚朴与生姜51个、紫苏叶与生姜75个。厚朴与紫苏叶、厚朴与生姜及紫苏叶与生姜等配伍后成分主要来源于分别为厚朴、生姜。复方成分种类主要源于3个单味药材的加和

而其挥发油成分主要来源于生姜。结论:半夏厚朴汤及配伍前后挥发性成分的数目及含量有一定的差异性

表明在煎煮过程中相关样品中挥发性成分溶解性发生变化或相互间产生了化学反应。

Abstract

Objective:To study the species and relative contents of volatile oils in the well-known Banxiahoupu Decoction and its related combinations and to explore the connections between the different compatibility of Banxiahoupu Decoctions and changes of volatile oils.Method: GC-MS method was used to analyze seven kinds of Banxiahoupu combinations: Banxiahoupu Decoction

Magnolia officinalis

Perilla frutescens

Zingiber officinale

Magnolia officinalis with Perilla frutescens

Magnolia officinalis with Zingiber officinale

Perilla frutescens with Zingiber officinale.Result:Differences were found in volatile oils: 54 oil in Banxiahoupu Decoction

44 in Magnolia officinalis

15 in Perilla frutescens

53 in Zingiber officinale

26 in compatibility of Magnolia officinalis and Perilla frutescens

51 in compatibility of Magnolia officinalis and Zingiber officinale

75 in compatibility P.frutescens and Zingiber officinale.Magnolia officinalis and Zingiber officinale contributed mostly to components of compatibility of Magnolia officinalis and Perilla frutescens

Magnolia officinalis and Zingiber officinale

as well as Perilla frutescens and Zingiber officinale

respectively.The volatile oils of Banxiahoupu decoction were a summation of components of Magnolia officinalis

Perilla frutescens and Zingiber officinale

and of which most components were identical with those in Zingiber officinale.Conclusion:[WTBZ] There is a great difference in species and relative contents of volatile oils beforo and-after compatibility

indicating the deliquescent of volatile components changed or certain chemical reactions taken place in the decoction process.

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