铨水大黄外观性状与所含5种蒽醌成分含量的关系

代婉莹; 孙维宏; 毛淑杰; 顾雪竹; 钮正睿; 李先端

doi:10.13422/j.cnki.syfjx.2009.09.031

您当前的位置：

首页 >

文章列表页 >

铨水大黄外观性状与所含5种蒽醌成分含量的关系

质量标准 | 更新时间：2024-09-23

- 铨水大黄外观性状与所含5种蒽醌成分含量的关系
- Relativity between the Contents of Five Anthraquinones and the Appearance of Rhubarb Produced in Quanshui Village
- 中国实验方剂学杂志 2009年15卷第9期页码：1-4
- 作者机构：
  
  1. 中国中医科学院中药研究所
  2. 甘肃神州红药材科技有限公司
- 作者简介：
- 基金信息：
  
  国家科郊部“十一五”支撑（2007BAI37B04）
- DOI：10.13422/j.cnki.syfjx.2009.09.031
  中图分类号： R284.1
- 纸质出版日期：2009
- 稿件说明：
移动端阅览
[1]代婉莹,孙维宏,毛淑杰,顾雪竹,钮正睿,李先端.铨水大黄外观性状与所含5种蒽醌成分含量的关系[J].中国实验方剂学杂志,2009,15(09):1-4.

DAI Wan-ying~1, SUN Wei-hong~2, MAO Shu-jie~1, et al. Relativity between the Contents of Five Anthraquinones and the Appearance of Rhubarb Produced in Quanshui Village[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(9): 1-4.
[1]代婉莹,孙维宏,毛淑杰,顾雪竹,钮正睿,李先端.铨水大黄外观性状与所含5种蒽醌成分含量的关系[J].中国实验方剂学杂志,2009,15(09):1-4. DOI： 10.13422/j.cnki.syfjx.2009.09.031.

DAI Wan-ying~1, SUN Wei-hong~2, MAO Shu-jie~1, et al. Relativity between the Contents of Five Anthraquinones and the Appearance of Rhubarb Produced in Quanshui Village[J]. Chinese journal of experimental traditional medical formulae, 2009, 15(9): 1-4. DOI： 10.13422/j.cnki.syfjx.2009.09.031.

摘要

目的:研究铨水大黄中5种蒽醌成分分析方法

对经经验鉴别认为优、劣分成商品等级的铨水大黄进行成分分析

探讨成分含量与外观性状的相关性。方法:色谱柱填料为Kromasil-C18（4.6 mm×150 mm

5μm）

检测波长254 nm。流动相∶甲醇-0.1%磷酸溶液（85∶15）。结果:30%糠芯大黄与正常大黄比较

5种蒽醌成分含量下降约30%左右。同株大黄的无糠芯部位和糠芯部位相比

成分含量相差达70%

0%左右。浅黄色大黄5种蒽醌成分含量较黄色大黄含量也低

结论:该方法重复性好

测定结果表明成分含量与经验鉴别优、劣的大黄有一定的相关性。

Abstract

Objective:To develop the analytical method of five anthraquinones contained in rhubarb produced in Quanshui Village.To investigated the relativity between the contents of five constituents and the appearance.Method:The HPLC method is as follows:Kromasil-C

column（4.6 mm×150 mm

particle diameter 5 μm）

detective wavelength is 254 nm

methanol-0.1% phosphonic acid solution（85∶15） as mobile phase.Results:Compared with the high-grade rhubarb

the content of five anthraquinones in inferior ones descented about 30%.Compared with the high-grade part

the content of five constituents in the inferior part of the same root tuber descented about 70～80%.The contents of five anthraquinones in pale yellow rhubarb were lower than that in yellow ones.Conclusion: The method with fine repeatability is suitable to evaluate the contents of anthraquinones in rhubarb and the results indicate the contents of five constituents are associated with the appearance.

关键词

Keywords

references

浏览量

118

下载量

CSCD

文章被引用时，请邮件提醒。

提交

工具集

关联资源

龟鹿补肾丸HPLC指纹图谱研究

葛根汤HPLC指纹图谱及多指标成分定量分析

滇重楼贮藏期间化学成分的变化

两面针商品药材的质量评价