芪参益智胶囊质量标准研究

肖新建

doi:10.13422/j.cnki.syfjx.2010.12.026

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芪参益智胶囊质量标准研究

化学与分析 | 更新时间：2024-09-23

- 芪参益智胶囊质量标准研究
- Studies on Quality Standard of Qishenyizhi Capsule
- 中国实验方剂学杂志 2010年16卷第12期页码：80-82
- 作者机构：
  
  泰安市中医医院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2010.12.026
  中图分类号： R286
- 纸质出版日期：2010
- 稿件说明：
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[1]肖新建.芪参益智胶囊质量标准研究[J].中国实验方剂学杂志,2010,16(12):80-82.

XIAO Xin-jian. Studies on Quality Standard of Qishenyizhi Capsule[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(12): 80-82.
[1]肖新建.芪参益智胶囊质量标准研究[J].中国实验方剂学杂志,2010,16(12):80-82. DOI： 10.13422/j.cnki.syfjx.2010.12.026.

XIAO Xin-jian. Studies on Quality Standard of Qishenyizhi Capsule[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(12): 80-82. DOI： 10.13422/j.cnki.syfjx.2010.12.026.

摘要

目的:建立芪参益智胶囊的质量标准。方法:采用薄层色谱法对芪参益智胶囊中党参、枸杞子、陈皮等进行定性鉴别;采用高效液相色谱法测定黄芪甲苷的含量。色谱柱:Agilent Hypersil ODS十八烷基键合硅胶柱（4.6 mm×250 mm

5μm）;流动相乙腈-水（32∶68）;流速1.0 mL·min-1;漂移管温度:45℃;气体流速1.5 L·min-1。结果:定性鉴别薄层色谱斑点清晰

阴性无干扰;黄芪甲苷在0.506～4.554μg呈良好线性关系;平均回收率为103.05%

RSD为1.43%（n=6）。结论:该方法简便、准确、可靠

可作为芪参益智胶囊的质量控制方法。

Abstract

Objective: To establish the quality standard of Qishenyizhi Capsule.Method: TLC were used to distinguish Dangshen

Pugongying

Zhizi and Chishao.HPLC were used for the deterimination of Astragaloside Ⅳ.The column was PHENOMENEX ODS C18（4.6 mm ×250 mm

5 μm）;the acetonitrile-water（35∶65） was used as mobile phase

the flow rate was 1.0 mL·min-1

the temperature of drift tube was 45 ℃ and the flow rate of N2 was 1.5 L·min-1.Result: The thin-layer chromatography spots were clear and the negative samples have no interferences;and astragaloside Ⅳ was linear in the range of 0.506～4.554 μg

and the average recovery was 103.05% with RSD 1.43%（n=6）.Conclusion: This method is simple

accurate

reliable and can be used as a quality control method for Qishenyizhi Capsule.

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