YUAN Jie1, LI Jing1, HUANG Song1, et al. Study on Quality Standard of Fuke Suppository[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(14): 68-70.
YUAN Jie1, LI Jing1, HUANG Song1, et al. Study on Quality Standard of Fuke Suppository[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(14): 68-70. DOI: 10.13422/j.cnki.syfjx.2010.14.037.
Objective:To study the qualitative standard of Fuke suppository
so as to better control the qual-ity of this product.Method:To establish the thin layer chromatography(TLC) for Rhizoma Coptidis
Cortex Phel-lodendri Chinensis
Radix Sophorae Flavescentis
Fructus Cnidii
and determination method for gentiopicrin by the high performance liquid chromatography(HPLC).Result:The TLC method could well identify Rhizoma Coptidis
Cortex Phellodendri Chinensis
Radix Sophorae Flavescentis
Fructus Cnidii
with clear spots
non-interference of negative controls and good specificity.Gentiopicrin was linear in the range of 0.688 ~ 6.880 μg
with a good corre-lation coefficient(r = 0.999 9).The average recovery is 101.91%
RSD as 2.00%(n = 6).Conclusion:This method is simple
reliable and precise
can be used for qualitative control of this preparation.