香椿中总黄酮提取工艺的研究

蔡定建; 梁晓鹏; 徐晶; 徐娜; 刘慧; 毛林春

doi:10.13422/j.cnki.syfjx.2010.15.019

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香椿中总黄酮提取工艺的研究

工艺与制剂 | 更新时间：2024-09-23

- 香椿中总黄酮提取工艺的研究
- Study on Methods of Extract and Determine of Flavonoid From Toona sinesis
- 中国实验方剂学杂志 2010年16卷第15期页码：31-33
- 作者机构：
  
  江西理工大学材料与化学工程学院
- 作者简介：
- 基金信息：
- DOI：10.13422/j.cnki.syfjx.2010.15.019
  中图分类号： R284
- 纸质出版日期：2010
- 稿件说明：
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[1]蔡定建,梁晓鹏,徐晶,徐娜,刘慧,毛林春.香椿中总黄酮提取工艺的研究[J].中国实验方剂学杂志,2010,16(15):31-33.

CAI Ding-jian, LIANG Xiao-peng, XU Jing, et al. Study on Methods of Extract and Determine of Flavonoid From Toona sinesis[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(15): 31-33.
[1]蔡定建,梁晓鹏,徐晶,徐娜,刘慧,毛林春.香椿中总黄酮提取工艺的研究[J].中国实验方剂学杂志,2010,16(15):31-33. DOI： 10.13422/j.cnki.syfjx.2010.15.019.

CAI Ding-jian, LIANG Xiao-peng, XU Jing, et al. Study on Methods of Extract and Determine of Flavonoid From Toona sinesis[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(15): 31-33. DOI： 10.13422/j.cnki.syfjx.2010.15.019.

摘要

目的:本文以香椿芽为原料

研究香椿芽中总黄酮的提取工艺。方法:采用碱提酸析法和微波辅助提取法成功地提取了香椿芽中的总黄酮。利用紫外分光光度法

以芦丁为对照品

NaNO2-Al（NO3）3-NaOH体系为显色剂测定香椿芽中总黄酮的含量。并利用L9（34）正交试验设计

确立了香椿芽中总黄酮的最佳提取条件及其产率。结果:最佳提取工艺为硼砂浓度0.5%

料液比1 g∶40 mL

提取30 min

提取温度60℃。结论:本试验可为香椿进一步研究和资源开发利用提供一定的科学依据。

Abstract

Objective: Flavonoids were extracted from Toona sinesis successfully.Method:Flavonoids were extract

By using the method of dissolved in alkali and separated out in acid and microwave.All the flavonoids in Toona sinesis were determined by UV-spectrophotometry with rutin as the standard and the quantities of flavonoids component were measured.And use L9（34） orthogonal test design.Result:It showed that the optimum extracting conditions were determined with 0.5%（M /V） Na2B4O7.10 H2O as extractor with the ratio of material to liquid at 1 g∶ 40 mL

and extracting for 30min /time and the separation temperature is 60 ℃.Conclusion:This study provided scientific basis for Toona sinesis

development and utilization of gardenia.

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