南、北五味子及其炮制品中木脂素类成分比较研究

楼招欢; 吕圭源; 陈素红

doi:10.13422/j.cnki.syfjx.2010.18.065

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南、北五味子及其炮制品中木脂素类成分比较研究

化学与分析 | 更新时间：2024-09-23

- 南、北五味子及其炮制品中木脂素类成分比较研究
- Comparative Study of Lignans Content in Two Kinds of Fructus Shisandrae and Its Processed Products
- 中国实验方剂学杂志 2010年16卷第18期页码：43-46
- 作者机构：
  
  1. 浙江中医药大学药物研究所
  2. 温州医学院
- 作者简介：
- 基金信息：
  
  国家十五重大科技专项“创新药物和中药现代化”（2003AA2Z3254）
- DOI：10.13422/j.cnki.syfjx.2010.18.065
  中图分类号： R284.1
- 纸质出版日期：2010
- 稿件说明：
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[1]楼招欢,吕圭源,陈素红.南、北五味子及其炮制品中木脂素类成分比较研究[J].中国实验方剂学杂志,2010,16(18):43-46.

LOU Zhao-huan1, LV Gui-yuan1, CHEN Su-hong2. Comparative Study of Lignans Content in Two Kinds of Fructus Shisandrae and Its Processed Products[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(18): 43-46.
[1]楼招欢,吕圭源,陈素红.南、北五味子及其炮制品中木脂素类成分比较研究[J].中国实验方剂学杂志,2010,16(18):43-46. DOI： 10.13422/j.cnki.syfjx.2010.18.065.

LOU Zhao-huan1, LV Gui-yuan1, CHEN Su-hong2. Comparative Study of Lignans Content in Two Kinds of Fructus Shisandrae and Its Processed Products[J]. Chinese journal of experimental traditional medical formulae, 2010, 16(18): 43-46. DOI： 10.13422/j.cnki.syfjx.2010.18.065.

摘要

目的:分析比较南、北五味子药材及炮制品中总木脂素以及五味子酯甲、甲素的含量。方法:①变色酸-浓硫酸比色法测定总木脂素含量;②高效液相色谱法测定五味子酯甲、甲素含量。结果:①生、制北五味子总木脂素含量在8.21%～9.60%和4.91%～7.09%之间

高于相应南五味子中的含量。②五味子酯甲在0.20～1.00μg、五味子甲素在0.387～1.94μg线性关系良好

酯甲回收率在95.7%～99.7%;甲素回收率在98.0%～103.7%;五味子酯甲和甲素的含量以南五味子为高者。结论:南、北五味子在总木脂素、五味子酯甲、甲素的含量上存在差异。含量测定方法准确可靠、重复性好

可用于五味子药材的质量控制。

Abstract

Objective:To analyse the difference of content of total lignanoid

wuweizi ester A and deoxy-schizandrin between Schisandra chinensis（Turcz.） Baill.and Schisandra sphenanthera Rehd.et Wils.Method:① Chromatometry with chromotropic acid and sulphuric acid as chromogenic agents was used to determine the total lig-nanoid;② HPLC was selected to determine the content of wuweizi ester A and deoxyschizandrin.Result: ① The content of total lignan in Schisandra chinensis was between 4.91%-93.60% and was twice higher than that in S.sphenanthera.② Schisantherin A and deoxyschizandrin were linear in the range of 0.20-1.00 μg and 0.387-1.94 μg respectively.The average recovery was 97.1% and 101.3% respectively.The content of schisantherin A and deoxyschizandrin in S.chinensis was lower than that in S.sphenanthera.Conclusion: There were differences on content of total lignanoid

wuweizi ester A and deoxyschizandrin between S.chinensis and S.sphenanthera.The HPLC method used for determination of wuweizi ester A and deoxyschizandrin was accurate and with good repeat-ability

and can be used to control the quality of Fructus Schisandrae.

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