正交试验优选枳实中辛弗林提取工艺

廖茂梁; 胡静; 尚海花; 王阳; 张铁军

doi:10.13422/j.cnki.syfjx.2011.13.025

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正交试验优选枳实中辛弗林提取工艺

工艺与制剂 | 更新时间：2024-09-23

- 正交试验优选枳实中辛弗林提取工艺
- Study on Extraction Technology of Synephrine in Citrus aurantium by Orthogonal Design
- 中国实验方剂学杂志 2011年17卷第13期页码：23-25
- 作者机构：
  
  1. 天津药物研究院
  2. 天津中医药大学
- 作者简介：
- 基金信息：
  
  天津市自然科学基金项目（10JCZDJC21400）
- DOI：10.13422/j.cnki.syfjx.2011.13.025
  中图分类号： R284
- 纸质出版日期：2011
- 稿件说明：
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[1]廖茂梁,胡静,尚海花,王阳,张铁军.正交试验优选枳实中辛弗林提取工艺[J].中国实验方剂学杂志,2011,17(13):23-25.

LIAO Mao-liang1, HU Jing2, SHANG Hai-hua1, et al. Study on Extraction Technology of Synephrine in Citrus aurantium by Orthogonal Design[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(13): 23-25.
[1]廖茂梁,胡静,尚海花,王阳,张铁军.正交试验优选枳实中辛弗林提取工艺[J].中国实验方剂学杂志,2011,17(13):23-25. DOI： 10.13422/j.cnki.syfjx.2011.13.025.

LIAO Mao-liang1, HU Jing2, SHANG Hai-hua1, et al. Study on Extraction Technology of Synephrine in Citrus aurantium by Orthogonal Design[J]. Chinese journal of experimental traditional medical formulae, 2011, 17(13): 23-25. DOI： 10.13422/j.cnki.syfjx.2011.13.025.

摘要

目的:研究枳实中辛弗林的最佳提取工艺。方法:以辛弗林的转移率为指标

考察了不同提取溶剂和提取方式对辛弗林提取率的影响

在此基础上采用正交试验设计

考察了加水量、煎煮温度、煎煮时间3个因素对辛弗林提取率的影响。结果:加水回流提取辛弗林的提取率较高

确定枳实的最佳提取工艺为:回流提取3次

提取1 h

加水依次为12

10倍量。结论:工艺条件简单

稳定

可行

辛弗林提取率高

为改进枳实的提取工艺提供了依据。

Abstract

Objective:To optimize the extraction process for synephrine in Citrus aurantium.Method: According to the yield rate of synephrine

the use of extraction solvent and distilling methods was studied.And L9（34） orthogonal design was used to determine the optimum extraction conditions.Three factors were studied as indexes that might affect the yield rate of synephrine

including water quantity

extraction temperature and time required.Result: The yield rate of synephrine in the water extraction was obviously higher than that in the other distilling methods.The optimized extraction procedure was as follows: refluxed three times

1.0 hour each time

the amount of water was 12

10 in turn.Conclusion: This extraction method is convenient and feasible

and can improve the extraction of synephrine from Citrus aurantium.

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